AOAC SPIFAN Nutrients ERP-Final Review (Dec. 2018)
2015.10 (Dec. 2018) Carn-07 MLT Report FOR ERP USE ONLY DO NOT DISTRIBUTE
Time, min
Flow rate, mL/min
Phase B, %
0
1.00 1.00 1.00 1.00 1.00 1.00
0 0
1.0 1.5 2.5 3.0 4.2
100 100
0 0
Table 2015.10C. LCMS parameters LCMS Settings* LCMS model Sciex 4000
Sciex 6500
Ionization mode IonSpray voltage
MRM 1000V 550ºC
MRM 2000V 550ºC
Turbo IonSpray Temp Entrance Potential (EP
10V
10V
Collision Gas (CAD) Nitrogen, 5.0
Nitrogen, 5.0 Nitrogen, 20.0 Nitrogen, 60.0 Nitrogen, 60.0 Y = 5 mm, X = 5 mm
Curtain Gas (CUR)
Nitrogen, 20.0
Nebulizing Gas (GS1) Nitrogen, 60.0 Nebulizing Gas (GS2) Nitrogen, 60.0
Needle Position
Y = 5 mm, X = 5 mm
Agilent 6490
LCMS model Ionization mode
MRM 380V
Fragmentor
Cell Accelerator Gas Temperature
5V
200ºC
Gas Flow Nebulizer
20 L/min 30 psi 225 ºC 1500V 500V 200V 100V 11 L/min
Sheath Gas Temp Sheath Gas Flow Nozzel Voltage + High Pressure RF + Low Pressure RF + LCMS model Ionization mode Capillary Voltage RF lens voltage Source Temp Nebulizer Temp Nebulizer Gas: Desolvation Gas: Capillary + API Gas
Waters TQD
MRM
2000 V 0.1eV 150ºC 450ºC
On
Nitrogen
900 L/hr, Nitrogen 50 L/hr, Nitrogen 0.25 mL/min Argon
Cone Gas: Collision Gas:
API Gas
On
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