2015.14 Vitamin B (July 2018)

2015.14 (JULY 2018) BVit‐02 Total Bs ERP Evaluation Form

FOR ERP USE ONLY DO NOT DISTRIBUTE

Table 6

Precision ‐ reproducibility

Conc. Level  (mcg/100g)

Product

SPIFAN Code

Analyte Nr. replicates (n)

REQUIREMENTS SMPR Conc. Level

RSD r

RSD R

RSD R ≤ Z %

Milk‐based Infant Formula Powder Soy‐based Infant Formula Powder

K16NTAV E10NWZC

B1 B1 B1 B1 B1 B1 B1 B1 B1 B1 B1 B1 B1 B1

mcg/100g RTF 

20 20 18 20 18 18 20 18 20 20 20 20 20 20

1.139

1.9

8.36

Repeatability Reproducibility

5%

1.1173 0.7642 0.7807 0.1752 0.4507 1.0348 0.0354 0.192

2.07 2.01 1.39 1.57 3.08

6.8

Milk‐based Partially Hydrolyzed Infant Formula Powder Soy‐based Partially Hydrolyzed Infant Formula Powder Adult Nutritional Ready‐to‐feed‐ High Fat Adult Nutritional Ready‐to‐feed‐ High Protein Milk‐based Child Formula Powder Progress Gold Milk‐based Infant Formula Stage 1 Powder Illuma Milk‐based Infant Formula Ready‐to‐feed

410057652Z 410457651Z 00729RF00 00730RF00 4052755861 4044755861 00866RF00 00859RF00 00795RF00 50350017W1 EV4H2R CLC10‐B

10%

13.15

6.62

23.41 18.22

2.2

7.99 8.88

2.04 4.22

17.39

SRM 1849a

1.368

4.4

8.84

Milk‐based Child Formula Powder Adult Low Fat Nutritional Powder Infant Elemental Formula Powder FOS/GOS‐based Infant Formula Powder

3.2149 1.9232

2.12 3.39 2.39 1.53

10.67

6.01 7.02 8.28

1.649

0.6045

Global Mean %

2.5

10.8

Conc. Level  (mcg/100g)

REQUIREMENTS SMPR Conc. Level

Product

SPIFAN Code

Analyte Nr. replicates (n)

RSD r

RSD R

RSD R ≤ Z %

Milk‐based Infant Formula Powder Soy‐based Infant Formula Powder

K16NTAV E10NWZC

B2 B2 B2 B2 B2 B2 B2 B2 B2 B2 B2 B2 B2 B2

mcg/100g RTF 

20 18 18 20 18 16 18 16 18 20 18 20 16 20

1.8253 1.3139 1.5317 0.9595 0.4846 0.3754 1.2452 1.6498

3.84 2.03 3.25 5.11 6.01 4.35 2.78 8.67 7.57 1.51 5.56 3.48 2.92 3.5

7.14 7.15 9.82 7.02 9.45 5.27 7.57 5.52

Repeatability Reproducibility

5%

Milk‐based Partially Hydrolyzed Infant Formula Powder Soy‐based Partially Hydrolyzed Infant Formula Powder Adult Nutritional Ready‐to‐feed‐ High Fat Adult Nutritional Ready‐to‐feed‐ High Protein Milk‐based Child Formula Powder Progress Gold Milk‐based Infant Formula Stage 1 Powder Illuma Milk‐based Infant Formula Ready‐to‐feed

410057652Z 410457651Z 00729RF00 00730RF00 4052755861 4044755861

10%

EV4H2R CLC10‐B

0.094

13.94

SRM 1849a a

2.1541 3.4014

7.57 4.89

Milk‐based Child Formula Powder Adult Low Fat Nutritional Powder Infant Elemental Formula Powder FOS/GOS‐based Infant Formula Powder

00866RF00 00859RF00 00795RF00 50350017W1

1.915

8.5

0.9181 1.2417

4.33 7.48

Global Mean %

4.3

7.5

Conc. Level  (mcg/100g)

REQUIREMENTS SMPR Conc. Level

Product

SPIFAN Code

Analyte Nr. replicates (n)

RSD r

RSD R

RSD R ≤ Z %

Milk‐based Infant Formula Powder Soy‐based Infant Formula Powder

K16NTAV E10NWZC

B3 B3 B3 B3 B3 B3 B3 B3 B3 B3 B3 B3 B3 B3

mcg/100g RTF 

20 20 20 20 18 18 20 18 18 20 20 20 20 20

8.4145 8.5906 6.6083 7.3954

3.01 2.47 5.48 3.32 1.79 4.01 3.34 1.44 4.22 2.52 4.38 1.42 1.64 3.1

7.83

Repeatability Reproducibility

5%

12.39

Milk‐based Partially Hydrolyzed Infant Formula Powder Soy‐based Partially Hydrolyzed Infant Formula Powder Adult Nutritional Ready‐to‐feed‐ High Fat Adult Nutritional Ready‐to‐feed‐ High Protein Milk‐based Child Formula Powder Progress Gold Milk‐based Infant Formula Stage 1 Powder Illuma Milk‐based Infant Formula Ready‐to‐feed

410057652Z 410457651Z 00729RF00 00730RF00 4052755861 4044755861

10%

8.28

10.21

4.148 3.072

5.4

4.78 8.22 9.47 4.86 5.02 8.93 7.42 9.16 6.25

4.5507 6.2518 0.9287 10.5432 10.6455 14.8004 12.9252 4.2641

EV4H2R CLC10‐B

SRM 1849a a

Milk‐based Child Formula Powder Adult Low Fat Nutritional Powder Infant Elemental Formula Powder FOS/GOS‐based Infant Formula Powder

00866RF00 00859RF00 00795RF00 50350017W1

Global Mean %

3.0

7.7

Conc. Level  (mcg/100g)

Product

SPIFAN Code

Analyte Nr. replicates (n)

REQUIREMENTS SMPR Conc. Level

RSD r

RSD R

RSD R ≤ Z %

Milk‐based Infant Formula Powder Soy‐based Infant Formula Powder

K16NTAV E10NWZC

B6 B6 B6 B6 B6 B6 B6 B6 B6 B6 B6 B6 B6 B6

mcg/100g RTF 

20 20 20 20 18 18 20 18 20 20 20 20 20 20

0.6467 0.6083

2.37 1.82 2.53 1.73 2.68 3.66 1.59 2.95 3.63 2.18 2.89 2.14 3.97 1.8

6.5

Repeatability Reproducibility

5%

4.63 8.86 3.66 4.37 3.93 4.24 4.95 4.57 5.48 16.77

Milk‐based Partially Hydrolyzed Infant Formula Powder Soy‐based Partially Hydrolyzed Infant Formula Powder Adult Nutritional Ready‐to‐feed‐ High Fat Adult Nutritional Ready‐to‐feed‐ High Protein Milk‐based Child Formula Powder Progress Gold Milk‐based Infant Formula Stage 1 Powder Illuma Milk‐based Infant Formula Ready‐to‐feed

410057652Z 410457651Z 00729RF00 00730RF00 4052755861 4044755861

10%

0.538

0.5358 0.4792 0.3727 0.3998 0.6549 0.0531 3.0907 1.9089 0.4932 0.3579 1.414

EV4H2R CLC10‐B

SRM 1849a a

Milk‐based Child Formula Powder Adult Low Fat Nutritional Powder Infant Elemental Formula Powder FOS/GOS‐based Infant Formula Powder

00866RF00 00859RF00 00795RF00 50350017W1

5.2

8.25 7.65

Global Mean %

2.6

6.4