September 2016 SPDS Book
Adulteration
• Non‐selective protein methods have fueled the potential to adulterate samples with non‐proteins and give inaccurate results • Melamine, urea, free amino acids cannot be differentiated using Kjeldahl, Dumas methods and have been the source of d l scan a s • Public health is still at risk; Economics still push adulteration
Existing Methods (Qualitative)
• Some proteins have FCC monographs. For example, Whey Protein is identified by testing for: – Ash – Fat – Lactose – Loss on drying – Nitrogen (and apply conversion factor) • DNA Analysis • LC/MS/MS
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