Expert Review Panel for Dietary Supplements

AOAC DECEMBER 2017 ERPs - METHOD REVIEW FORM

Submission Date

2017-12-07 17:12:28

AOAC Expert Review Panel: Method Review

Reviewer Information Required to validate your review.

Name

John Szpylka

E-mail

john.szpylka@mxns.com

Organization

Merieux NutriSciences

Remember, the main purpose of your review is to ensure the method conforms to the applicable SMPR. View and download SMPRs here:

SPDS SMPRs SPSFAM SMPRs

Method Review

Title of Method

Determination of Mitragynine in Mitragyna speciosa Raw Materials and Finished Products

AOAC Candidate Method Number (e.g. ALN-01)

KRA-002

Applicable SMPR

2015.008

I. Summary of the Method

I. Summary of the Method

The analytes of interest are extracted from powder samples using acetic acid/methanol/water and from liquid finished products using methanol. Separation and quantitation is performed by HPLC/UV using a C18 column with gradient mobile phase conditions.

II. Review of the Method Only: