AOAC SPIFAN Stakeholder Panel (August 25, 2018)

Background

• Working group launched in March 2017 (WG chair: Jan Kuhlmann, SGS, Germany) • AOAC SMPR 2017.017 approved by SPIFAN in Sep 2017 • Call for methods issued – 2 methods received • Expert Review Panel (ERP) meetings: • March 2018: Recommendations for the methods to obtain AOAC First Action Official Method SM status • July 2018: Both methods adopted as the AOAC First Action Official Methods SM

SMPR: 3-MCPD

Parameter

3-MCPD * in dry infant formula samples (powder)

3-MCPD* in liquid infant formula samples

Analytical range (ʅŐ/kg)

25 – ш ϭϬϬϬ

3 – ш ϭϮϬ

LOQ (ʅg/kg)

ч Ϯϱ

ч ϯ

Accuracy (%)

70-125

70-125

ч ϮϮ

ч ϮϮ

% RSD r

25-100 ʅg/kg ч ϰϰ

% RSD R

ч ϰϰ

хϭϬϬ ʅg/kg

ч Ϯϱ

* Total analyte content expressed as free 3-MCPD resulting either from separate or from combined determination of free 3-MCPD and bound 3-MCPD.