Basic Training 4th Annual ICP Conference
17.20 Method Validation
Following The ISO Guide 34 Guidelines should result in a dependable CRM.
• ISO begins with a solid foundation of a Validated Method. • They build on it with the additional support of QC Samples • ISO then requires the creation of an error budget for determining Uncertainty. • All of this builds to yield a Certified Value with it’s Uncertainty. • So why might there be a need to make this even more robust?
CerAfied Value
Uncertainty
Q C
Validated Method (based on NaAonal Standard )
17.21 Method Validation
Two independent methods are better than one .
• What if the CRM is method specific? • Using two methods validated by two independent National Standard CRMs solidifies that foundation. • Each method has it’s own series of QC samples. • Each methods requirs the creation of an Uncertainty Budget. • There is one final step...
Cer Certified Value Uncertainty Budget Uncertainty Budget Q C Q C Validated Method Validated Method
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