SPIFAN Stakeholder Panel (September 23, 2017)

Specific Performance Claims-II 3-MCPD* in dry infant formula (powder) in liquid infant formula samples Analytical range 25 – 1000 μg/kg 3 – 120 μg/kg LOD N/A N/A LOQ d 25 μg/kg d 3 μg/kg 2-MCPD* in dry infant formula (powder) in liquid infant formula samples Analytical range 25 – 500 μg/kg 3 – 60 μg/kg LOD N/A N/A LOQ d 25 μg/kg d 3 μg/kg Glycidol** in dry infant formula (powder) in liquid infant formula samples Analytical range 15 – 400 μg/kg 2 – 48 μg/kg LOD N/A N/A LOQ d 15 μg/kg d 2 μg/kg * Analyte content resulting either from separate or from combined determination of free and bound analyte. **Analyte content resulting from the determination of bound glycidol.

Specific Performance Claims-III 3-MCPD* in dry infant formula (powder)

in liquid infant formula

Accuracy

70 -125 %

70 -125 %

RSD r RSD R

d 22 %

d 22 % d 44 %

25-100 μg/kg: d 44 % > 100 μg/kg: d 25 %

2-MCPD* Accuracy

in dry infant formula (powder)

in liquid infant formula

70 -125 %

70 -125 %

RSD r RSD R

d 22 %

d 22 % d 44 %

25-100 μg/kg: d 44 % > 100 μg/kg: d 25 %

Glycidol **

in dry infant formula (powder)

in liquid infant formula

Accuracy

70 -125 %

70 -125 %

RSD r RSD R

d 22 %

d 22 % d 44 %

15-48 μg/kg: d 44 % > 48 μg/kg: d 25 %