AOAC ERP Gluten Assays - Dec 2018

Table A-3. Raw concentration data in mgg/kg gluten for blind duplicates from 19 participants using the Quadratic curve fitting for calculation; data presented were calculated from the mean of two replicates on the plate per sample; part 1 for samples 1 - 10; outliers are marked as c for Cochran, g for Grubbs, dg for double Grubbs.

Lab

1

2

3

4

5

6

7

8

9

10

A B C D

11.6 7.6 9.9 11.7 15.5 11.0 0.2 1.9

65.4 63.8 34.4 42.6 2.1 54.4 62.9 33.1 13.5 0.7 64.7 71.4 30.9 28.7 3.4 59.5 64.2 31.7 33.1 4.6 58.2 53.9 34.5 31.7 4.8 59.7 65.2 36.4 35.4 7.3 68.0 73.0 34.6 40.6 7.3 63.1 74.6 39.2 39.9 6.9 63.9 64.0 31.0 35.9 1.2 55.2 52.7 25.7 26.3 1.7 70.0 67.1 29.4 36.8 4.8 63.2 65.5 35.4 38.1 2.3 58.9 59.4 39.2 37.3 2.1 60.5 60.8 35.2 29.6 0.8 74.4 71.8 40.5 40.0 2.6

2.1 4.5 7.8 31.1 32.1 49.4 57.1 0.9 5.1 13.0 22.5 30.7 46.6 35.1 3.2 9.4 7.6 24.3 22.7 43.3 39.4 3.7 5.2 7.5 30.0 26.3 51.8 51.5 6.3 9.0 6.0 32.7 29.4 42.2 48.6 7.0 5.0 5.1 31.5 33.2 46.1 50.3 8.1 64.6 9.6 45.0 48.8 67.3 50.7 8.8 7.3 8.3 43.7 47.3 63.8 62.6 2.6 7.4 5.9 41.5 39.2 52.4 56.8 2.7 5.6 4.8 24.8 57.7 45.6 48.8 1.4 8.6 6.7 25.7 28.0 42.2 45.1 4.5 7.5 9.0 35.3 31.8 49.6 53.8 3.0 7.1 6.4 41.5 29.2 49.4 43.2 1.9 9.9 8.8 33.5 33.9 51.5 42.5 0.8 6.1 5.6 34.0 27.5 52.9 47.3 1.6 6.7 8.6 40.1 37.4 50.5 53.6

6.5 8.7 9.9g -0.4g 10.4 14.3 7.5 11.2 15.8 6.6

8.9 -0.5 -0.6 7.0 0.4 0.3

9.0 10.5 10.0 11.2 8.9 11.1 0.5 4.9 9.1 7.7 13.3 15.8 10.5 10.0 0.3 0.2 12.3 10.4 12.9 13.9 10.0 10.6 3.5 -0.2 10.0 8.9 12.4 17.0 12.8 11.0 0.2 0.5 12.6 11.0 15.5 13.5 12.9 14.5 0.6 2.3 12.6 8.0 14.5 15.2 10.9 13.6 0.3 0.9 9.9 9.1 18.9 12.9 9.7 13.2 0.4 0.8

116.8c 56.1c 46.9 29.0 37.0c 14.1c 12.1 6.6 26.1 40.5 60.0 29.4

E F

G H

I

J

K

10.5 4.6 11.8 9.2

8.8

8.4 0.6c 19.2c 53.0 60.6 60.4 55.0 0.6

L

8.9 14.6 12.0 13.5 21.9g 20.2g 0.5 0.9

76.3 65.5 33.9 26.6 6.0c 0.4c 11.4 7.0 48.0 36.5 47.4 54.5

M

9.2 10.2 12.9 10.8 7.7

7.6 1.3 0.3 9.6 1.1 0.6 8.6 1.4 0.5 7.8 1.2 3.0 9.9 2.4 0.6

N O

9.2 9.5 15.8 9.9

8.4

11.3 11.4 12.5 14.1 11.2 10.1 6.4 12.1 13.8 13.7 12.0 10.2 15.7 14.8 9.3

P

68.4 56.4 29.2 36.2 2.8c 9.6c 12.9 4.5 33.1 22.9 51.9 66.6

Q R U

9.8 9.5 9.6 13.2 7.5 10.5 1.4 0.4 7.9 14.1 13.4 13.9 13.0 14.6 2.4 3.6

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