AOAC ERP Gluten Assays - Dec 2018

Table A-4. Raw concentration data in mgg/kg gluten for blind duplicates from 19 participants using the Quadratic curve fitting for calculation; data presented were calculated from the mean of two replicates on the plate per sample; part 2 for samples 11 - 21; outliers are marked as c for Cochran, g for Grubbs, dg for double Grubbs.

Lab

11

12

13

14

15

16

17

18

19

20

21

A 2.1 5.2 19.2 15.4 13.1 23.8 42.2 28.00 3.4 0.3 10.7 7.3 14.0 13.6 18.3 12.4 5.0 3.3 6.0 16.8 22.2 22.4 B 1.1 0.7 21.5 19.8 13.5 12.0 35.0 21.64 0.3 -0.1 2.6 1.3 11.2 6.5 25.1 12.8 6.4 5.3 7.9 10.2 14.7 12.5 C 1.5 1.5 20.8 13.1 8.5 7.8 17.7 12.84 3.8 1.6 1.9 4.5 7.1 10.8 7.5 18.2 3.3 5.5 10.0 10.9 19.1 15.5 D 2.6 3.6 11.6 20.2 8.8 13.7 22.6 19.86 13.4c 0.7c 8.5 9.7 18.0 8.4 28.0 25.9 8.2 2.6 12.7 15.1 17.1 22.3 E 1.3 1.6 32.6 24.6 11.2 18.4 21.0 24.23 0.6 0.5 4.1 8.3 13.3 6.5 23.4 26.2 6.7 5.4 10.1 9.4 21.5 19.1 F 5.2 1.3 18.5 13.7 18.7 26.9 29.0 18.91 1.3 -0.5 3.5 3.5 7.1 12.2 20.9 25.7 8.5 4.5 12.3 12.9 21.0 21.1 G 1.3 1.5 18.4 18.9 12.2 11.4 23.1 22.46 0.7 3.8 4.0 6.4 10.1 6.9 22.9 21.7 7.0 11.1 11.7 14.8 20.8 19.8 H 3.3 2.0 22.0 42.1 20.4 18.6 41.3 43.53 3.0 3.9 7.1 14.1 20.5 35.9 30.0 28.7 7.0 8.1 15.7 20.8 35.8dg 28.3dg I 2.8 2.2 38.7 17.4 18.5 18.9 34.9 40.50 0.9 1.2 9.6 6.6 12.1 32.8 24.7 33.5 6.7 9.2 17.5 19.5 39.6dg 32.4dg J 2.1 1.3 23.6 37.2 14.4 21.7 27.9 28.48 7.7 1.1 2.9 3.6 14.8 15.1 17.2 35.0 5.7 10.7 15.2 11.6 21.8 19.8 K 3.5 1.3 20.9 25.6 27.2 11.9 27.7 23.33 0.4 3.0 3.7 4.6 17.9 4.5 9.2 14.7 4.7 4.2 10.1 15.4 19.3 16.6 L 1.5 1.5 18.9 28.5 13.3 13.5 42.2 26.77 0.8 0.8 5.7 3.3 8.7 9.8 40.9 28.7 4.1 6.1 13.6 12.4 19.9 21.5 M 1.2 1.5 12.5 21.3 13.3 7.5 28.7 20.78 0.4 0.6 1.5 3.2 3.4 11.2 26.3 13.5 4.3 3.1 14.9 9.7 16.5 12.3 N 1.7 1.3 20.6 12.7 11.2 16.3 26.1 32.64 1.9 0.6 3.2 6.1 14.4 6.8 29.9 15.1 4.3 4.1 8.2 17.9 16.6 20.5 O 2.1 3.0 19.2 19.3 10.4 13.6 20.1 34.33 0.5 6.9 5.3 6.3 12.3 8.8 14.6 16.6 5.1 4.9 11.3 9.8 19.8 22.2 P 5.1 8.1 21.4 17.8 23.1 26.2 33.6 27.99 9.8g 3.8g 3.4 17.5 12.3 12.6 36.2 21.3 7.6 10.9 13.3 14.6 21.6 22.4 Q 7.6 3.3 14.9 15.8 17.2 24.0 32.5 19.66 3.8 0.9 4.4 3.9 11.5 6.3 20.0 13.8 7.5 10.8 12.2 11.9 26.7 22.3 R 3.8 1.0 24.0 19.0 11.0 13.5 31.6 22.28 0.3 2.7 4.6 3.1 12.5 8.6 22.0 24.7 6.5 6.8 9.9 12.5 19.2 17.3 U 2.2 1.8 22.5 21.3 20.9 12.5 24.7 38.32 0.8 0.8 5.2 5.7 18.2 12.9 21.5 31.8 7.6 9.3 19.0 14.8 21.2 24.0

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