SPDS SET 2: ASH-01

NATURAL REMEDIES PVT LIMITED QUALITY CONTROL DEPARTMENT

Acquired by Sample Name

: Admin

: Withania somnifera ext

Sample ID

: RM - RD / 1162

Vail #

: 20

Injection Volume Data File Name Method File Name Batch File Name Report File Name Data Acquired Data Processed

: 20 uL

: Quan007.lcd

: Withaina.met.lcm : Batch 01.lcb : Calibration.lcr

: 1/15/2007 12:35:34 PM : 1/23/2007 2:53:34 AM

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Quan007.lcd

mV

1Det.A Ch1

125

3

100

1

75

50

5

2

4

25

6

0

0

5

10

15

20

25

30

35

40

45

min

Det.A Ch1/227nm 1

Detector A Ch1 227nm Peak # Ret. Time

Area

Height

Area %

Name

1 2 3 4 5 6 Total

15.545 19.701 20.375 21.378 22.239 25.523

405115 290787 833061 202935 220542 41941 1994381

71109 41508 118930 35689 38625 7689 313550

20.313 14.580 41.770 10.175 11.058 2.103 100.000

Withanoside IV Withanoside V Withaferin A 12- Deoxy withastramonolide

Withanollide A Withanolide B

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Quan007.lcd