SPDS SET 2: ASH-01

QUALITY CONTROL DEPARTMENT

Name of Sample Method Name Data File Name

: Withania somnifera : RD - 1170 : C:\Methods\WITHANIA.met

: D:\LC10-ATvp\2007\Method validation\Apr 2007\020407\S6-Rep2

Vial No

: 10007

Injection Volume

: 20

Date & Time

: 4/4/07 5:08:37 PM

0.4

0.3

23.917

17.225

23.050

0.2

Volts

21.392

0.1

27.058

0.0

22.083

0

5

10

15

20

25

30

35

40

45

Minutes

Detector A - 1 (227nm)

Pk # Retention Time Name

Area Area Percent

1 2 3 4 5 6

17.225 21.392 22.083 23.050 23.917 27.058

WIthanoside IV Withanoside V

1080249 742686 2475863 978751 1255922 289554

15.83 10.88 36.29 14.34 18.41

Withaferin A

Withastramonolide

Withanolide A Withanolide B

4.24

Totals

6823025

100.00