SPDS SET 2: ASH-01

QUALITY CONTROL DEPARTMENT

Name of Sample Method Name Data File Name

: Withania somnifera : RD - 1170 : C:\Methods\WITHANIA.met

: D:\LC10-ATvp\2007\Method validation\Apr 2007\020407\S6-Rep3

Vial No

: 10007

Injection Volume

: 20

Date & Time

: 4/4/07 5:54:29 PM

0.4

0.3

23.917

17.225

23.050

0.2

Volts

21.375

0.1

27.058

0.0

22.092

0

5

10

15

20

25

30

35

40

45

Minutes

Detector A - 1 (227nm)

Pk # Retention Time Name

Area Area Percent

1 2 3 4 5 6

17.225 21.375 22.092 23.050 23.917 27.058

WIthanoside IV Withanoside V

1075861 740290 2484320 965956 1260234 292481

15.78 10.86 36.43 14.17 18.48

Withaferin A

Withastramonolide

Withanolide A Withanolide B

4.29

Totals

6819142

100.00