SPDS SET 2: ASH-01

NATURAL REMEDIES PVT LIMITED QUALITY CONTROL DEPARTMENT

Acquired by Sample Name

: Admin

: Withania : std mix

Sample ID

: Dilution : III

Vail #

: 10

Injection Volume Data File Name Method File Name Batch File Name Report File Name Data Acquired Data Processed

: 20 uL

: Lin016.lcd

: Withaina.met.lcm : Batch 01.lcb : Calibration.lcr

: 1/14/2007 12:03:10 PM : 1/23/2007 2:08:01 AM

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Lin016.lcd

mV

1Det.A Ch1

4

750

6

5

3

500

250

1

2

0

0

5

10

15

20

25

30

35

40

45

min

Det.A Ch1/227nm 1

Detector A Ch1 227nm Peak # Ret. Time

Area 1275513 1146136 4332623 4800626 4137256 4196971 19889126

Height

Area %

Name

1 2 3 4 5 6 Total

15.539 19.721 20.383 21.394 22.253 25.530

203131 163005 635519 804013 688329 726582 3220579

6.413 5.763

Withanoside IV Withanoside V Withaferin A 12- Deoxy withastramonolide

21.784 24.137 20.802 21.102 100.000

Withanollide A Withanolide B

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Lin016.lcd