AOAC SPIFAN ERP Meeting Book-March 16, 2016

VitK-01 MEF FOR ERP USE ONLY DO NOT DISTRIBUTE

Table 3

Precision ‐ repeatability.

RSDr

RSD iR

RSDr

RSD iR

Product

SPIFAN Code Analyte

Nr. replicates (n) Conc. Level

Conc. Level

REQUIREMENTS SMPR

SRM 1849a

6 Vit K1 7 Vit K1 8 Vit K1 9 Vit K1 10 Vit K1 11 Vit K1 12 Vit K1 13 Vit K1 14 Vit K1 15 Vit K1 16 Vit K1 17 Vit K1

8 7 8 9 9 8 9 9 8 9 8 8

11.5

6.3

X

≤ Z % ≤ W %

Adlt. Nutr Powd, Milk based

3.3

13.0 Analyte 1 11.2 Analyte 2 6.1 Analyte 3 11.0 Analyte 4 6.3 Analyte 5 7.1 Analyte 1 11.0 Analyte 2 3.9 Analyte 3 8.6 Analyte 4 5.4 Analyte 5 5.0 Analyte 1 Analyte 2 Analyte 3 Analyte 4 Analyte 5 Analyte 1 Analyte 2 Analyte 3 Analyte 4 Analyte 5

1‐10

8% or less

Inf. Form Powd, Partially Hydrolyzed Milk Based Inf. Form Powd, Partially Hydrolyzed Soy Based

7

8.1 2.6 2.6 8.3 6.1 6.5 9.1 8.5

Adlt. Nutr Powd, Low fat

Child Form. Powd

Infant Elemental Powd

>10

5% or less

Infant Formula Powd Milk Based Infant Formula Powd Soy Based

Inf Form RTF Milk Based

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat

10.5

Global Mean % #DIV/0!

7.9

SPIFAN ERP X Checklist v 1.0