AOAC SPIFAN Review Team Meeting Book-July 22, 2015

BVIT-02 FOR ERP/WORKING GROUP USE ONLY DO NOT DISTRIBUTE

Tabel 1: Total B6 SPIFAN I results (ppb)

Day 1

Day 2

Day 3

%RSD

PYR PAL

13870 13939 13190 13114 13537 13177

2.7 6.1 3.9 2.7 3.0 8.8 3.0 2.9 5.3 3.0 1.1 1.3 2.8 6.1 2.7 1.1 4.8 1.5 2.0 2.2 2.4 6.4 5.6 2.3 2.8 2.9 2.6 1.4 3.1 2.4 2.0 8.4 1.9 2.4

450 666

440 655

414 679

391 645

413 630

387 608

SRM 1849a

PAM Total

14995 15043 14292 14158 14588 14180 22191 22128 21648 21438 20762 20718

PYR PAL

161 170

154 162

132 161

124 165

137 142

132 136

10.2

Adult pwd (MP)

PAM Total

22525 22447 21943 21729 21043 20988

PYR PAL

4984 90.6 5554 5737 64.8 61.3 5864 476

5072 90.4 5639 5802 65.5 57.8 5926 473

4714

4810 67.7 5376 5695 39.3 39.6 5775 495

4754 94.4 5299 5730 53.4 27.5 5812 447

4781 64.7 5277 5632 53.2 40.2 5726 428

87

15.6

Infant pwd (hydro MB)

PAM Total

446

5251 5647 54.5 35.8 5738

PYR PAL

17.4 30.0

Infant pwd (hydro SB)

PAM Total

PYR PAL

17304 17872 18300 18577 18613 17897

60.9 141

56.2 159

48.1 155

41

66.6 145

50

17.2

Adult pwd (lowfat)

PAM Total

135

144

17507 18089 18505 18754 18826 18092 14732 14857 14536 14528 14620 14927

PYR PAL

141 93.6

137

150 67.4

144 90.6

142 76.5

130 98.3

Child pwd

PAM Total

103.7

15.6

14969 15100 14756 14765 14841 15157

PYR PAL

4903 46.3 22.6 4972 6083 7111 6146 49.8 6259 915 17.7 52.5 986 3903 55.1 3958 4655 46.3 60.7 4763 62 622 396

4870 32.8 4921 5991 7077 6103 49.2 43.9 6197 942 17.3 54.4 1014 3791 60.9 3852 4708 32.8 55.6 4797 18 623 453

4773 29.3 20.9 4824 6412 7551 6300 39.3 34.2 6374 675 453 49.4 1034 3750 49.8 3800 4969 29.3 46.3 5045 966 18

4740 32.7 17.6 4791 6216 7295 6011 28.2 27.8 6067 960 17.6 52.6 1031 3841 49.6 3891 4786 32.7 40.4 4860 604 465

4981 46.1 5048 6232 7280 6396 40.2 44.6 6481 988 17.6 52.3 1058 3684 58.7 3743 4663 46.1 49.5 4759 20 600 438

4959 55.2 16.4 5031 6261 7278 6463 49.7 38.6 6552 968 17.9 51.6 1038 3813 56.6 3870 4757 55.2 43.6 4857 554 454

25.4 12.0

Infant pwd (elemental)

PAM Total

PYR PAL

Infant pwd (MB)

PAM Total

PYR PAL

25.8 20.0

Infant pwd (SB)

PAM Total

PYR PAL

Infant RTF

PAM Total PAL PAM Total PYR

Adult RTF (HP)

PYR PAL

25.4 15.4

Adult RTF (HF)

PAM Total

2.2

3