AOAC SPIFAN Review Team Meeting Book-July 22, 2015

BVIT-02 FOR ERP/WORKING GROUP USE ONLY DO NOT DISTRIBUTE

Table 3. Precision data for Milk-based IF Day 1 Day 2 Day 3

Day 4

Day 5

Day 6

% RSD

3862 3869 4038

3685 3695 3676

3500 3494 3653

3642 3679 3760

3699 3690 3633

3946 3916 3752

PYR

569 580 551 216 210 206

559 590 576

552 573 591 105

560 594 591 112 116 113

560 567 563 112 117 110

565 629 592 107 110 107

PAL

99 99 90

PAM

80

112

Total B 6 Average

3.4

4701

4358

4221

4390

4351

4576

11622 11741 11896

11830 11540 11747

11459 11415 11619

11310 11910 11838

11666 11319 11263

11833 11899 11882

THI

1.4

Total THI Average

11753

11706

11498

11686

11416

11871

11082 10970 11065

11119 11361 11272

10681 10739 10681

11371 11224 11367

11425 11061 11383

10894 11008 10961

RIB

2.2

Total RIB Average

11039

11251

10700

11321

11290

10954

Table 4. Spike recoveries of Non-phosphorylated Vitamins in Placebo product. Day 1 Day 2 Day 3

Average

Pyr Pal

107.3 102.2 102.2 100.4 98.5 94.7 101.9 103.8 100.4 97.9

98.7 100 98.6 98.4 99.3 93.1

89.3 106.5

98.5 102.9 100.3 99.2 99.2 95.4 101.9 104.4 100.7 99.6

Spike Level 1

Pam Thi Rib Pyr Pam Thi Rib Pal

100 98.8 99.8 98.4

100.3 105.6 102.1

103.6 103.8 99.6 100.8

Spike Level 2

100

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