13-Cis Retinyl Palmitate/Acetate as RE
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mcg/100g RTF
15
30
49.4227
4.2602
7.4548
8.62
15.08
0.84
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mcg/100g RTF
13
26
16.2217
1.7461
3.4600
10.76
21.33
1.00
1
14
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
15
30
1.4391
0.0671
0.1303
4.66
9.06
0.30
JMQT233 DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based mcg/100g RTF
15
30
7.8940
3.2636
3.4367
41.34
43.54
1.85
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mcg/100g RTF
15
30
2.5268
0.4850
0.5759
19.20
22.79
0.81
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mcg/100g RTF
12
24
16.1120
0.4843
2.1751
3.01
13.50
0.63
2 & 3
14
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mcg/100g RTF
15
30
8.5529
1.4362
2.0574
16.79
24.06
1.03
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mcg/100g RTF
15
30
13.7327
0.8805
1.7236
6.41
12.55
0.57
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mcg/100g RTF
14
28
11.7489
0.1408
1.2573
1.20
10.70
1.35
9
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mcg/100g RTF
15
30
16.9437
0.5518
1.7938
3.26
10.59
0.50
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mcg/100g RTF
15
30
3.8708
0.9107
1.1576
23.53
29.91
1.14
Trans Retinyl Palmitate/Acetate as RE
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mcg/100g RTF
15
30
352.38
12.6081
25.1273
3.58
7.13
0.53
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mcg/100g RTF
14
28
453.99
22.0834
48.0814
4.86
10.59
0.82
14
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
15
30
5.05
0.1506
0.3959
2.98
7.84
0.31
JMQT233/DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based mcg/100g RTF
15
30
43.35
22.3361
22.3361
51.52
51.52
2.82
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mcg/100g RTF
15
30
43.23
7.3704
9.7070
17.05
22.45
1.22
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mcg/100g RTF
12
24
51.28
1.4784
6.0266
2.88
11.75
0.65
2 & 3
14
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mcg/100g RTF
15
30
39.00
6.0814
8.3122
15.59
21.32
1.15
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mcg/100g RTF
15
30
48.83
3.7347
4.6842
7.65
9.59
0.53
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mcg/100g RTF
14
28
54.83
0.6812
3.2122
1.24
5.86
0.33
9
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mcg/100g RTF
14
28
40.30
0.3237
2.4155
0.80
5.99
0.32
9
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mcg/100g RTF
15
30
44.48
6.4568
6.8880
14.52
15.49
0.86
Total Retinyl Palmitate/Acetate as RE
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mcg/100g RTF
15
30
401.80
14.9957
31.3624
3.73
7.81
0.59
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mcg/100g RTF
14
28
471.35
22.2689
49.5985
4.72
10.52
0.82
14
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
15
30
6.49
0.2118
0.5206
3.26
8.02
0.33
JMQT233/DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based mcg/100g RTF
15
30
51.25
25.5187
25.5187
49.80
49.80
2.80
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mcg/100g RTF
15
30
46.34
7.6934
10.4773
16.60
22.61
1.25
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mcg/100g RTF
12
24
67.39
1.5484
8.0413
2.30
11.93
0.69
2 & 3
14
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mcg/100g RTF
15
30
47.55
7.5035
10.3302
15.78
21.73
1.20
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mcg/100g RTF
15
30
62.56
4.2798
6.0407
6.84
9.66
0.56
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mcg/100g RTF
14
28
66.58
0.7492
4.3338
1.13
6.51
0.38
9
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mcg/100g RTF
14
28
57.34
0.6089
4.1275
1.06
7.20
0.41
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mcg/100g RTF
15
30
48.35
7.3132
7.8551
15.13
16.25
0.91
d: Alpha Tocopherol Acetate
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mg/100g RTF
15
30
6.06
0.1489
0.3732
2.46
6.16
0.70
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mg/100g RTF
15
30
4.61
0.1438
0.3048
3.12
6.61
0.73
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
14
28
172.89
3.3739
14.9913
1.95
8.67
0.58
9
JMQT233/DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based
mg/100g RTF
13
26
1.55
0.1081
0.1253
6.97
8.08
0.76
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mg/100g RTF
14
28
12.73
0.4888
0.9263
3.84
7.28
0.93
14
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mg/100g RTF
15
30
1.80
0.0657
0.2025
3.65
11.25
1.07
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mg/100g RTF
13
26
1.84
0.0388
0.1561
2.11
8.50
0.81
9
15
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mg/100g RTF
14
28
1.30
0.0217
0.0842
1.67
6.47
0.58
9
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mg/100g RTF
13
26
1.44
0.0206
0.0667
1.43
4.62
0.42
9
14
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mg/100g RTF
13
26
1.56
0.0094
0.0648
0.60
4.15
0.38
9
14
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mg/100g RTF
15
30
1.79
0.0606
0.1192
3.38
6.66
0.63
dL Alpha Tocopherol
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mg/100g RTF
15
30
2.59
0.2027
0.4661
7.82
17.99
1.81
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mg/100g RTF
13
26
5.96
0.1955
0.4178
3.28
7.01
0.80
13 & 14
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
14
28
36.38
2.1032
4.5387
5.78
12.47
1.87
14
JMQT233/DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based
mg/100g RTF
15
30
0.34
0.1489
0.1658
43.66
48.62
3.64
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mg/100g RTF
14
28
0.58
0.0230
0.0525
3.99
9.10
0.93
14
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mg/100g RTF
11
22
0.48
0.0080
0.0569
1.67
11.94
0.92
1 -3
14
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mg/100g RTF
14
28
0.14
0.0124
0.0607
8.90
43.56
2.81
1
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mg/100g RTF
14
28
0.46
0.0361
0.0400
7.89
8.74
0.68
14
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mg/100g RTF
13
26
0.49
0.0077
0.0279
1.57
5.68
0.44
9
14
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mg/100g RTF
14
28
0.45
0.0117
0.0350
2.59
7.73
0.60
14
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mg/100g RTF
14
28
0.41
0.0637
0.0718
15.48
17.44
1.34
14
Total Vitamin E as TE
Total number
of
laboratories
Total number
of replicates
Overall mean
of all data
(grand mean)
Repeatability
standard
deviation
Reproducibility
standard
deviation
Repeatability
relative
standard
deviation
Reproducibility
relative standard
deviation
HORRAT
value
Cochran's Test
Single Grubbs
Test
Units
p
Sum(n(L))
XBARBAR
s(r)
s(R)
RSD(r)
RSD(R)
Ppractice Sample 1
810637
Wyeth Nutri Global Control
mg/100g RTF
15
30
5.98
0.1955
0.3886
3.27
6.50
0.74
Ppractice Sample 2
DDP 2 - 2013
Nestle DDP 2 - 2013 P-Test
mg/100g RTF
12
24
7.50
0.1230
0.4014
1.64
5.35
0.63
8 & 13 & 14
EKVJ578 VJKY373
CLC10-b
SRM 1849a
mg/Kg
12
24
209.24
4.0620
8.1769
1.94
3.91
0.27
9
13 & 15
JMQT233/DQDF457
1172572116
Infant Formula Powder Partial Hydrolyzed Milk Based
mg/100g RTF
14
28
1.87
0.1458
0.2246
7.79
12.01
1.15
9
LARU224 GLVC238
11750017V3
Adult Nutritional Powder Milk Protein Based
mg/100g RTF
14
28
13.30
0.4972
0.9545
3.74
7.17
0.93
14
ADVZ021 LUJP087
117257651Z
Infant Formula Powder Partially Hydrolyzed Soy Based mg/100g RTF
15
30
2.27
0.1240
0.2307
5.46
10.15
1.00
SNPZ056 CBNJ010
00394RF00
Adult Nutritional Powder Low Fat
mg/100g RTF
14
28
1.95
0.0528
0.2104
2.71
10.78
1.04
9
MNGN284 EPXW887
E29JVLV
Infant Formula Powder Soy Based
mg/100g RTF
14
28
1.79
0.0370
0.0754
2.07
4.22
0.68
9
ZNP1092 YKLP059
D04HTCVV
Infant Formula Powder Milk Based
mg/100g RTF
14
28
1.94
0.0256
0.0800
1.32
4.13
0.40
9
MOPG098 SJLQ035
SPIFAN Milk Control
Infant Formula RTF Milk Based
mg/100g RTF
14
28
2.01
0.0163
0.0772
0.81
3.84
0.37
9
FRZK569 FHTX798
00403RF00
Infant Elemental Powder
mg/100g RTF
15
30
2.22
0.1046
0.1233
4.70
5.55
0.55
Outliers (Labs removed)
Outliers (Labs removed)
Outliers (Labs removed)
Outliers (Labs removed)
Outliers (Labs removed)
Outliers (Labs removed)
