2. AOACRIChemContMethods-2018Awards

496  M astovska et al . : J ournal of AOAC I nternational V ol . 98, N o . 2, 2015

Table 6. Collaborative study results (in µg/kg) obtained by the participating laboratories in blind duplicates fortified at the low PAH level in mussel Laboratory No. PAH Sample ID 1 2 3 4 5 6 7 8 9 10 1,7-DMP SFC M1 40.8 41.5 44.4 23.9 45.4 39.2 40.9 44.5 30.9 37.9 SFC M6 18.2 47.1 51.3 25.9 44.4 38.9 43.2 43.8 29.0 31.6 1-MN SFC M1 17.0 21.2 23.2 10.4 19.1 17.5 22.1 24.6 16.2 16.0 SFC M6 27.9 16.5 27.6 12.6 18.9 18.8 21.2 20.2 16.8 18.6 1-MP SFC M1 33.7 a 8.3 9.9 5.7 10.4 9.6 10.4 10.8 9.5 13.1 SFC M6 18.0 a 8.0 10.7 6.6 10.1 10.1 10.9 11.0 10.6 10.8 2,6-DMN SFC M1 21.8 9.5 13.8 12.3 14.8 11.7 13.4 14.5 11.8 12.0 SFC M6 17.8 10.8 14.6 16.5 14.8 12.4 11.9 15.7 11.0 14.6 3-MC SFC M1 6.4 10.4 10.5 8.0 10.2 10.6 11.0 10.9 8.9 11.4 SFC M6 6.1 8.1 11.3 10.2 10.0 10.8 11.1 10.8 8.8 11.8 Ant SFC M1 4.9 4.4 3.1 1.2 2.3 5.0 4.7 4.9 3.8 4.9 SFC M6 4.6 3.6 3.6 1.5 2.3 5.0 4.8 5.2 3.6 4.5 BaA SFC M1 3.9 4.7 4.0 2.5 4.1 4.6 4.6 4.7 3.9 5.2 SFC M6 4.2 4.0 4.9 3.1 4.1 4.5 4.7 4.5 3.8 5.1 BaP SFC M1 1.3 2.1 1.8 1.0 1.3 0.1 b 1.8 1.9 1.5 1.6 SFC M6 1.4 2.0 1.9 1.2 1.2 0.1 b 1.8 1.8 1.3 1.6 BbF SFC M1 4.4 5.3 4.8 3.9 4.8 4.9 4.8 4.8 4.0 5.6 SFC M6 4.7 4.3 5.1 4.7 4.7 4.3 4.8 4.7 4.1 5.7 BghiP SFC M1 1.8 2.3 a 2.0 1.7 2.0 2.0 2.0 2.1 1.7 2.3 SFC M6 1.7 1.7 a 2.2 2.0 1.9 2.0 2.2 1.9 1.7 2.3 BkF SFC M1 1.8 1.8 2.2 1.6 2.0 1.8 1.9 2.1 47.0 a 2.5 SFC M6 1.8 1.9 2.1 2.0 1.9 2.0 1.8 2.0 1.6 a 2.1 Chr SFC M1 12.7 14.5 14.3 11.7 14.6 14.4 14.3 14.9 12.9 16.9 SFC M6 13.2 12.3 15.3 14.2 14.3 14.4 14.4 14.0 12.9 17.0 DBahA SFC M1 1.7 2.2 2.0 1.5 1.8 1.9 1.9 1.9 2.1 2.2 SFC M6 1.7 1.7 1.9 1.7 1.8 1.8 1.9 1.8 1.6 2.2 Fln SFC M1 5.3 6.2 5.6 5.5 5.1 5.1 5.0 5.1 4.5 6.2 SFC M6 5.2 6.4 5.7 6.1 5.0 5.3 4.8 5.2 4.6 5.9 Flt SFC M1 8.9 10.1 9.9 19.5 b 10.0 12.4 9.6 10.2 10.8 12.0 SFC M6 11.0 8.1 10.9 20.7 b 9.7 12.5 9.8 9.8 7.5 11.2 IcdP SFC M1 1.8 2.4 1.9 1.6 2.0 1.9 1.9 2.0 1.9 2.3 SFC M6 1.6 1.9 2.1 1.9 2.0 2.0 2.0 1.9 1.7 2.4 Naph SFC M1 20.3 a 27.6 26.7 20.2 23.1 20.2 26.2 26.4 23.8 14.8 SFC M6 36.0 a 28.9 30.6 18.7 23.3 20.9 26.5 23.2 23.9 20.8 Phe SFC M1 15.8 27.5 b 14.2 12.7 15.2 14.2 14.5 15.3 14.1 21.2 b SFC M6 13.9 26.7 b 15.6 14.3 14.9 14.5 14.8 15.4 12.9 17.5 b Pyr SFC M1 14.9 14.4 14.7 11.8 14.5 13.7 14.1 14.7 13.0 16.8 SFC M6 14.2 11.9 15.4 13.2 14.2 14.0 14.4 14.0 12.9 16.8

a Outliers removed by the Cochran test. b  Outliers removed by single Grubbs’ test.