Review Team (February 2016)

BVit-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Quantitative Analysis Summary Report

Batch Data Path Analysis Time

D:\MassHunter\Data\2015\January\Vitamins\01 WSV-Val\QuantResults\01-01-2015-WSV-VAL-LOQ-1.batch.bin

Analyst Name Reporter Name

1/21/2015 3:45 PM 1/21/2015 3:46 PM 1/21/2015 3:45 PM

PC-PC\Harisenthil PC-PC\Harisenthil

Report Time

Last Calib Update

Batch State

Processed

2015-01-21T15:45:19.8773503+05:30

2015-01-21T15:46:15.0745074+05:30

2015-01-21T15:45:19.6763388+05:30

Sequence Table Data File STANDARD-1 ppb.d STANDARD-2 ppb.d STANDARD-5 ppb.d STANDARD-10 ppb.d STANDARD-20 ppb.d STANDARD-50 ppb.d

Acq Method File

Sample Name

Sample Type Position

Volume Level

VITAMINS-B-2-12-14.m STANDARD-1 ppb VITAMINS-B-2-12-14.m STANDARD-2 ppb VITAMINS-B-2-12-14.m STANDARD-5 ppb VITAMINS-B-2-12-14.m STANDARD-10 ppb VITAMINS-B-2-12-14.m STANDARD-20 ppb VITAMINS-B-2-12-14.m STANDARD-50 ppb

Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration

P1-A2 P1-A3 P1-A4 P1-A5 P1-A6 P1-A7 P1-A8 P1-A9 P1-B1 P1-B2 P1-B3

5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00

1 2 3 4 5 6 7 8 9

STANDARD-100 ppb.d VITAMINS-B-2-12-14.m STANDARD-100 ppb STANDARD-200 ppb.d VITAMINS-B-2-12-14.m STANDARD-200 ppb STANDARD-300 ppb.d VITAMINS-B-2-12-14.m STANDARD-300 ppb STANDARD-400 ppb.d VITAMINS-B-2-12-14.m STANDARD-400 ppb STANDARD-500 ppb.d VITAMINS-B-2-12-14.m STANDARD-500 ppb

10 11

Quantitation Results Target Compound

Thiamine

Sample Type

Response

Final Conc

Exp Conc

Accuracy

Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration Calibration

931

3.8702 4.1758 5.8424 7.5134 17.6007 42.5437 92.9638 197.0627 308.9452 403.0980 499.4873

2096 8454

5.0000

116.85

14828 53306

20.0000

88.00

148451 340779 737865 1164642 1523789 1891466

100.0000 200.0000 300.0000 400.0000 500.0000

92.96 98.53

102.98 100.77

99.90

Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample Sample

1589 1723 1560 1960 1743 2070 1657 1842 1941 1593 6713 5799 6610 6210 5818 6825 5260 6382 5980 5978

4.0427 4.0779 4.0351 4.1400 4.0833 4.1688 4.0605 4.1092 4.1351 4.0437 5.3861 5.1465 5.3591 5.2543 5.1513 5.4155 5.0051 5.2994 5.1938 5.1935 7.5731 7.7208 7.4439 7.7456

15056 15619 14563 15714

Page 1 of 53 TUV-SUD South Asia, Bangalore

01-01-2015-WSV-VAL-Linearity.xlsx

Printed at: 5:50 PM on: 2/18/2015