Review Team (February 2016)

Amino-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

RT Sig Lvl Amount Area Rsp.Factor Ref ISTD # Compound [μM] -------|-|--|----------|----------|----------|---|---|-|------------------- 6.877 1 1 1.00000 5.84492 1.71089e-1 No No 1 Lysine 2 5.00000 27.45505 1.82116e-1 3 12.50000 81.90633 1.52613e-1 4 25.00000 125.07404 1.99882e-1 5 50.00000 213.28142 2.34432e-1 6.985 1 1 1.00000 3.60393 2.77475e-1 No No 1 Tyrosine 2 5.00000 19.08224 2.62024e-1 3 12.50000 50.68980 2.46598e-1 4 25.00000 95.27022 2.62411e-1 5 50.00000 175.77512 2.84454e-1 7.178 1 1 1.00000 3.94819 2.53281e-1 No No 1 Methionine 2 5.00000 18.35064 2.72470e-1 3 12.50000 50.21463 2.48931e-1 4 25.00000 89.24659 2.80123e-1 5 50.00000 161.04089 3.10480e-1 7.378 1 1 1.00000 5.67687 1.76153e-1 No No 1 Valine 2 5.00000 18.80631 2.65868e-1 3 12.50000 49.32087 2.53442e-1 4 25.00000 81.68585 3.06051e-1 5 50.00000 142.32000 3.51321e-1 7.544 1 1 25.00000 88.56639 2.82274e-1 No Yes 1 Norvaline 2 25.00000 87.19655 2.86709e-1 3 25.00000 98.12215 2.54784e-1 4 25.00000 82.15121 3.04317e-1 5 25.00000 72.62400 3.44239e-1 8.369 1 1 1.00000 3.78179 2.64425e-1 No No 1 Isoleucine 2 5.00000 18.05161 2.76984e-1 3 12.50000 50.89798 2.45589e-1 4 25.00000 86.14241 2.90217e-1 5 50.00000 152.65004 3.27547e-1 8.486 1 1 1.00000 3.74597 2.66954e-1 No No 1 Leucine 2 5.00000 17.92867 2.78883e-1 3 12.50000 50.03949 2.49803e-1 4 25.00000 84.72035 2.95088e-1 5 50.00000 150.09650 3.33119e-1 8.629 1 1 1.00000 3.81862 2.61875e-1 No No 1 Phenyl Alanine --------------------------------------------------------------------- --------------------------------------------------------------------- Peak Sum Table --------------------------------------------------------------------- ***No Entries in table*** --------------------------------------------------------------------- 4 Warnings or Errors : 2 5.00000 19.32251 2.58766e-1 3 12.50000 51.62406 2.42135e-1 4 25.00000 96.05376 2.60271e-1 5 50.00000 177.97539 2.80938e-1

Warning : Overlapping peak time windows at 6.794 min, signal 1 Warning : Overlapping peak time windows at 6.877 min, signal 1 Warning : Overlapping peak time windows at 8.369 min, signal 1 Warning : Overlapping peak time windows at 8.486 min, signal 1 UPLC-DAD 7/31/2015 5:54:40 PM Vikas Kanase

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