AOAC OMB Final Action Recommendation (December 2019)-2016.14

2016.14 (October 2019) – FOS-03 METHOD

FOR ERP USE ONLY DO NOT DISTRIBUTE

= ( × 0.9) +

320

321

= glucose concentration in Solution B (in µg/mL), C FB

= Fructose concentration in

where C GB

Solution B (in µg/mL), D = dilution factor between Solution A and Solution B (from Table

322

2016.14C ), V A

323

= total volume of Solution A (in mL), m A

= mass of sample weighed to prepare

324

Solution A (in g), 0.0001 = factor to convert analyte concentration in solution (in µg/mL) to

325

analyte concentration in sample (in g/100 g), 0.9 = factor to correct for uptake of water during

326

fructan hydrolysis.

(d) For samples requiring the blank correction adapt the above equations as follows:

327

= ( − 0 ) × × � � × 0.0001 = ( − 0 ) × × � � × 0.0001

328

329

330

where C G0

= glucose concentration in Blank Solution B (in µg/mL), C F0

= Fructose concentration in

331

Blank Solution B (in µg/mL).

(e) For samples requiring result in g/100 g original product (powder or liquid concentrate) that have

332

been subjected to reconstitution as described in H(a) , adapt the above equations, as follows:

333

= × × � � × � + � × 0.0001 = × × � � × � + � × 0.0001 = ( − 0 ) × × � � × � + � × 0.0001 = ( − 0 ) × × � � × � + � × 0.0001

334

335

336

337

17

Made with FlippingBook HTML5