AOAC OMB Final Action Recommendation (December 2019)-2016.14

2016.14 (October 2019) – FOS-03 MANUSCRIPT

FOR ERP USE ONLY DO NOT DISTRIBUTE

1 Table 2016.14F. HPAEC-PAD gradient for CarboPac PA1 analytical column (or equivalent) 2

Flow rate, mL/min

200 mM NaOH, % A

Water, % B

1 M NaOAc, % C

Time, min

0.0

0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25

7.5 7.5

92.5 92.5 75.0 75.0 30.0 30.0 60.0 92.5 92.5

0.0 0.0 0.0 0.0

13.0 14.1 20.0 21.0 28.0 30.0 31.0 43.0

25.0 25.0 40.0 40.0 40.0

30.0 30.0

0.0 0.0 0.0

7.5 7.5

3

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