AOAC OMB Final Action Recommendation (December 2019)-2016.14

2016.14 (October 2019) – FOS-03 MANUSCRIPT

FOR ERP USE ONLY DO NOT DISTRIBUTE

1 Table 3. Statistical evaluation of results from determination of fructans in the practice 2 sample a 3

Requirements (SMPR 2014.002)

≤ 6 %

≤ 12 %

Sample name

n b

Mean, g/100 g

RSD r

, % RSD R

, %

Child formula powder d Child formula powder e

9 c

0.266 d 0.242 e

2.53 d 1.63 e

6.70 d 9.16 e

7

a Results are reported in g/100 g of product as reconstituted (25 g product + 200 g water). 4 b Number of laboratories considered in the evaluation. 5 c Lab 11 eliminated because of single analysis. Lab 14 data obtained on Day 1 taken into account. 6 d Results obtained with satisfactory batches of sucrase enzyme mixture. 7 e Results obtained with unsatisfactory batch (B) of sucrase enzyme mixture.

8 9 10

58