Amino-01 (July 2018)

Amino‐01 (July 2018) Method Evaluation Form (MEF)

0.632 0.623 0.745 0.719

0.028 0.037 ‐0.085 ‐0.059 ‐0.024 0.070

 FOR ERP USE ONLY DO NOT DISTRIBUTE

Mean   

0.684 0.070

SD   

Reference Material

Measured Results

T stat Bias

Difference from  certified value

Confidence interval 

CRM product

Analyte

Certified value Uncertainty Certified range Concentration

p ‐value

Nominal

1.264 1.269 1.258 1.198 1.272 1.262 1.239 1.280 1.270 1.246 1.255 1.275 1.242 1.214 1.265 1.256 1.251 1.275 1.255 1.265 1.057 1.100 1.205 1.106 1.083 1.104 1.077 1.091 1.056 1.049 1.055 1.115 1.184 1.101 1.074 1.097 1.089 1.093 1.036 1.062 0.595 0.591 0.557 0.540 0.599 0.587 0.572 0.595 0.612 0.581 0.591 0.593 0.548 0.547 0.597 0.586 0.576 0.592 0.610 0.591 1.167 1.170 1.176 1.159 1.180 1.162 1.169 1.217 1.174 1.153 1.162 1.177 1.165 1.164

‐0.003 ‐0.008 0.003 0.063 ‐0.011 ‐0.001 0.022 ‐0.019 ‐0.009 0.015 0.006 ‐0.014 0.019 0.047 ‐0.004 0.005 0.010 ‐0.014 0.006 ‐0.004 0.005 0.020 ‐0.047 ‐0.090 ‐0.195 ‐0.096 ‐0.073 ‐0.094 ‐0.067 ‐0.081 ‐0.046 ‐0.039 ‐0.045 ‐0.105 ‐0.174 ‐0.091 ‐0.064 ‐0.087 ‐0.079 ‐0.083 ‐0.026 ‐0.052 ‐0.082 0.041 ‐0.015 ‐0.011 0.023 0.040 ‐0.019 ‐0.007 0.008 ‐0.015 ‐0.032 ‐0.001 ‐0.011 ‐0.013 0.032 0.033 ‐0.017 ‐0.006 0.004 ‐0.012 ‐0.030 ‐0.011 ‐0.003 0.020 0.028 0.025 0.019 0.036 0.015 0.033 0.026 ‐0.022 0.021 0.042 0.033 0.018 0.030 0.031

NIST 1849A

Leucine

1.261

0.05

1.211 ‐ 1.311

‐0.005

1.194

0.247

1.246 ‐ 1.265

Mean   

1.256 0.020

SD   

Reference Material

Measured Results

T stat Bias

Difference from  certified value

CRM product

Analyte

Certified value Uncertainty Certified range Concentration

Confidence interval 

p ‐value

Nominal

NIST 1849A

Lysine

1.01

0.071

0.939 ‐ 1.081

0.082

8.809

0.000

1.072 ‐ 1.111

Mean   

1.092 0.041

SD   

Reference Material

Measured Results

T stat Bias

Difference from  certified value

CRM product

Analyte

Certified value Uncertainty Certified range Concentration

Confidence interval 

p ‐value

Nominal

NIST 1849A

Phenylalanine

0.58

0.021

0.559 ‐ 0.601

0.003

0.657

0.519

0.573 ‐ 0.593

Mean   

0.583 0.020

SD   

Reference Material

Measured Results

T stat Bias

Difference from  certified value

CRM product

Analyte

Certified value Uncertainty Certified range Concentration

Confidence interval 

p ‐value

Nominal

NIST 1849A

Proline

1.195

0.086

1.109 ‐ 1.281

‐0.024

6.650

0.000

1.164 ‐ 1.179

SPIFAN ERP Checklist v 1.6

27.06.2013