Amino-01 (July 2018)
Amino-01 (JULY 2018) 180124 AA SPIFAN SLV Appendices A-I
FOR ERP USE ONLY DO NOT DISTRIBUTE
Single Laboratory Validation Report for Total Amino Acids by UHPLC-UV in Infant Formulas and Adult Nutritionals -– APPENDICES (A to I) Appendix E : reproducibility performance requirements for each analyte/sample pair according to the concentration of the analyte in the reconstituted product.
SPIFAN II SLV kit product
Analyte
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
His
8% 5% 8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8% 5% 8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8% 5% 5% 5% 8% 5% 5% 5% 5% 5% 5% 5% 8% 8% 5% 5% 5% 5%
5% 5% 5% 5% 8% 5% 5% 5% 5% 5% 5% 5% 8% 5% 5% 5% 5% 5%
8% 5% 8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8%
8%
8% 8% 8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8%
8%
8% 5% 8% 8% 5% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8%
8%
8%
8% 8% 8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8%
8% 8% 5% 5% 8% 5% 5% 5% 5% 5% 5% 5% 8% 8% 5% 5% 5% 5%
5% 8% 5% 5% 8% 5% 5% 5% 5% 5% 5% 5% 8% 5% 5% 5% 5% 5%
Tau Ser Arg Gly Asp Glu Thr Ala Pro Lys Tyr
11%
11%
11%
11%
11%
11%
11%
11%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 5% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 5% 8%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
8% 8% 8% 8% 5% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8% 8%
xCys Met
Val
Ile
Leu Phe
Those reproducibility performance requirements were set for each analyte/matrix pair according to the concentration of the analyte in mg/100 g reconstituted product (Appendix A) and the SMPR*. Colors are used for clarity. * updated version proposed by the amino acid working group to be reviewed by the stakeholder panel during the August 2018 annual meeting.
Jaudzems, Guthrie, Lahrichi, and Fuerer – January 2018
page 5/22
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