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Table 1

Accuracy - Spike Recovery

Avg (%)

RSD % Avg (%) RSD (%)

Infant Powder Milk

D04HTCVV

choline (ion)

3 days x duplicates

16.6

101.3% 2.0% 97.8% 1.7%

Infant Powder Soy

E29JVLV

choline (ion)

3 days x duplicates

19.1

95.8% 5.2% 92.8% 6.7%

Infant Pwd Milk Part Hyd

1172572116

choline (ion)

3 days x duplicates

17.6

95.7% 5.8% 96.8% 3.5%

Infant Pwd Soy Part Hyd

117257651Z

choline (ion)

3 days x duplicates

17.1

94.0% 6.2% 98.8% 4.4%

Adult Powder Low Fat

00394RF00

choline (ion)

3 days x duplicates

17.3

97.0% 6.4% 98.9% 3.2%

Adult Pwd Milk

11750017V3

choline (ion)

3 days x duplicates

3.91

59.2% 32.8%

90.5% 6.9%

Adult Pwd Milk

(repeat)

choline (ion)

3 days x duplicates

3.74

80.3%

7.0% 94.1%

9.6%

Child Formula Pwd

00412RF00

choline (ion)

3 days x duplicates

5.44

104.1% 0.7% 100.3% 6.0%

Infant Elemental Pwd

00403RF00

choline (ion)

3 days x duplicates

8.42

99.2% 3.0% 100.1% 2.3%

Infant RTF Milk

SPIFAN CTL

choline (ion)

3 days x duplicates

21.42

102.2% 4.7% 99.3% 4.0%

Adult RTF HP

00414RF00

choline (ion)

3 days x duplicates

48.35

102.4% 7.7% 101.1% 2.4%

Adult RTF HF

00406RF00

choline (ion)

3 days x duplicates

53.20

104.2% 4.3% 97.4% 2.8%

MEAN 99.6%

97.3%

Infant Powder Milk

D04HTCVV

carnitine (ion)

3 days x duplicates

1.71

98.3% 2.2% 96.2% 2.4%

Infant Powder Soy

E29JVLV

carnitine (ion)

3 days x duplicates

0.898

97.4% 1.0% 98.6% 1.9%

Infant Pwd Milk Part Hyd

1172572116

carnitine (ion)

3 days x duplicates

1.12

99.6% 4.1% 98.0% 4.7%

Infant Pwd Soy Part Hyd

117257651Z

carnitine (ion)

3 days x duplicates

1.01

96.8% 1.6% 98.9% 1.7%

Adult Powder Low Fat

00394RF00

carnitine (ion)

3 days x duplicates

0.00

102.3% 3.4% 99.4% 1.1%

Adult Pwd Milk

11750017V3

carnitine (ion)

3 days x duplicates

0.00

100.6% 0.6% 98.8% 0.6%

Child Formula Pwd

00412RF00

carnitine (ion)

3 days x duplicates

5.39

100.2% 2.1% 97.5% 4.2%

Infant Elemental Pwd

00403RF00

carnitine (ion)

3 days x duplicates

1.51

100.2% 3.4% 95.5% 3.2%

Infant RTF Milk

SPIFAN CTL

carnitine (ion)

3 days x duplicates

2.68

99.7% 4.0% 95.8% 4.0%

Adult RTF HP

00414RF00

carnitine (ion)

3 days x duplicates

15.50

97.3% 1.6% 98.7% 1.7%

Adult RTF HF

00406RF00

carnitine (ion)

3 days x duplicates

21.64

97.5% 4.8% 98.0% 2.0%

MEAN 99.1%

97.8%

Infant Powder Milk

D04HTCVV

acetylcarnitine

3 days x duplicates

1.69

103.0%

90.7%

Infant Powder Soy

E29JVLV

acetylcarnitine

3 days x duplicates

0.90

96.7%

95.3%

Infant Pwd Milk Part Hyd

1172572116

acetylcarnitine

3 days x duplicates

1.10

94.9%

91.1%

Infant Pwd Soy Part Hyd

117257651Z

acetylcarnitine

3 days x duplicates

1.00

94.6%

91.1%

Adult Powder Low Fat

00394RF00

acetylcarnitine

3 days x duplicates

0.00

98.5%

95.8%

Adult Pwd Milk

11750017V3

acetylcarnitine

3 days x duplicates

0.00

95.9%

97.0%

Child Formula Pwd

00412RF00

acetylcarnitine

3 days x duplicates

5.42

97.5%

98.0%

Infant Elemental Pwd

00403RF00

acetylcarnitine

3 days x duplicates

1.53

96.6%

89.5%

Infant RTF Milk

SPIFAN CTL

acetylcarnitine

3 days x duplicates

2.65

101.5%

98.4%

Adult RTF HP

00414RF00

acetylcarnitine

3 days x duplicates

15.5

92.5%

98.2%

Adult RTF HF

00406RF00

acetylcarnitine

3 days x duplicates

21.5

98.0%

95.3%

MEAN 97.2%

94.6%

+80% native

Spike Recovery

Product

Nr. replicates (n)

Native level

mg/100g as RTF

Analyte

+ 40% Native

SPIFAN Code

SPIFAN ERP Checklist v1.0

Carn-05 MEF Form

FOR ERP USE ONLY

DO NOT DISTRIBUTE