484 / 620
Table 1
Accuracy - Spike Recovery
Avg (%)
RSD % Avg (%)
RSD (%)
Child Formula Powder Lot#00847RF00
Thiamine
6
ND and < LOD 107.4
4.1
95.3
1.2
(duplicate on
101.3
96.9
each of 3 days)
94.3
3.2
100.5
1.3
98.6
102.4
99.9
0.4
99.0
1.5
99.4
96.9
Global Mean % 100.1
2.6
98.5
1.3
Child Formula Powder Lot#00847RF00
Riboflavin
6
102.70
95.9
1.3
91.1
0.3
(duplicate on
94.1
90.7
each of 3 days)
99.7
0.5
95.3
1.9
100.5
92.8
94.9
3.6
96.7
1.5
90.1
94.7
Global Mean % 95.9
2.0
93.6
1.3
Child Formula Powder Lot#00847RF00
Nicotinic acid
6
ND
93.7
0.0
95.5
0.4
(duplicate on
93.7
95.0
each of 3 days)
102.4
3.9
107.2
0.2
108.2
107.6
94.5
5.0
103.3
3.0
101.4
99.0
Global Mean % 99.0
2.7
101.3
1.2
Child Formula Powder Lot#00847RF00
Nicotinamide
6
ND
108.1
0.6
101.6
2.3
(duplicate on
107.2
104.9
each of 3 days)
109.1
0.6
108.4
0.7
108.2
109.6
109.1
0.1
109.5
0.7
108.9
108.3
Global Mean % 108.4
1.0
107.1
1.2
Child Formula Powder Lot#00847RF00
Pantothenic acid
6
48.05
101.1
2.8
92.0
4.7
(duplicate on
97.1
98.4
each of 3 days)
96.0
0.3
93.2
0.9
96.4
94.4
92.8
3.0
96.4
0.2
96.9
96.2
Global Mean % 96.7
1.8
95.1
1.8
Child Formula Powder Lot#00847RF00
Pyridoxine
6
ND
101.9
1.3
94.1
4.4
(duplicate on
100.1
100.1
each of 3 days)
97.2
3.6
96.7
0.6
92.3
95.8
97.9
0.2
91.2
0.1
97.6
91.0
Global Mean % 97.8
1.7
94.8
1.7
Child Formula Powder Lot#00847RF00
Pyridoxal
6
5.76
100.2
1.6
93.1
4.3
(duplicate on
97.9
98.9
each of 3 days)
95.2
1.9
95.6
0.0
92.6
95.6
95.1
0.5
99.6
4.1
94.4
94.0
Global Mean % 95.9
1.4
96.1
2.5
Child Formula Powder Lot#00847RF00
Pyridoxamine
6
1.71
103.9
2.1
94.3
1.5
(duplicate on
100.8
92.4
each of 3 days)
101.7
2.1
97.9
1.6
98.7
95.6
100.6
1.6
93.4
2.9
102.9
97.2
Global Mean % 101.4
1.8
95.1
2.1
Child Formula Powder Lot#00847RF00
Biotin
6
ND
98.4
1.5
95.4
3.1
(duplicate on
100.6
99.6
each of 3 days)
98.7
1.4
94.1
1.3
100.6
95.8
104.5
1.7
98.7
1.4
107.0
100.6
Global Mean % 101.6
1.6
97.4
2.0
Infant Elemental Powder Lot#00796RF
Thiamine
6
ND
105.3
2.5
101.4
0.6
(duplicate on
101.7
100.5
each of 3 days)
95.5
4.1
95.3
1.7
90.2
93.0
96.7
1.2
98.1
0.3
95.1
98.6
Global Mean % 97.4
2.6
97.8
0.9
Infant Elemental Powder Lot#00796RF
Riboflavin
6
ND
91.9
2.1
95.0
0.1
(duplicate on
94.7
94.9
each of 3 days)
97.9
2.9
97.2
3.2
94.0
93.0
102.8
4.6
100.9
0.5
96.3
101.7
Global Mean % 96.2
3.1
97.1
1.2
Infant Elemental Powder Lot#00796RF
Nicotinic acid
6
ND
104.2
0.4
106.8
1.3
(duplicate on
103.6
104.8
each of 3 days)
95.9
0.1
94.6
2.1
95.7
91.8
99.3
2.9
106.6
2.6
SPIFAN Code
+ Spike Level 2
Spike Recovery
Product
Nr. replicates (n)
Native level
(mcg/100g)
Analyte
+ Spike Level 1
SPIFAN ERP Checklist v1.0
BVit-01 - MEF FORM
FOR ERP USE ONLY
DO NOT DISTRIBUTE