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Standard Overall (n = 5)

Thiamine

Riboflavin

Niacin Nicotinic Acid Pyridoxal

Pyridoxamine Pyridoxine

Recovery (%)

99.2

99.6

98.3

100.5

104.4

101.3

100.9

RSD (%)

3.5

6.6

5.9

7.3

15.4

7.2

2.3

Recovery (%)

100.4

99.9

100.8

99.1

97.9

100.3

98.8

RSD (%)

3.2

4.9

5.1

4.7

10.2

3.5

1.6

Recovery (%)

100.3

100.3

101.2

100.0

95.3

97.5

100.0

RSD (%)

2.1

3.7

3.2

2.2

10.7

4.6

1.3

Recovery (%)

100.5

100.6

100.5

100.4

104.3

99.8

100.4

RSD (%)

2.2

3.4

3.4

2.6

9.9

3.6

2.0

Recovery (%)

99.6

99.6

99.3

99.8

98.9

100.7

99.9

RSD (%)

2.4

1.9

2.5

1.8

10.9

4.0

1.4

Recovery (%)

100.1

100.1

100.2

100.0

100.1

99.8

100.0

RSD (%)

2.2

1.1

3.0

1.8

8.7

3.2

1.1

WS5

WS6

Table 5a. Determination of linearity – average concentration recovery of independent standards run as samples on five separate days (N=5)

WS1

WS2

WS3

WS4

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