602-603 / 620
Table 1
Accuracy - Spike Recovery
Avg (%)
RSD % Avg (%)
RSD (%)
Adult Nutritional RTF High Fat, placebo
00820RF00
Total B1
3 days x 2 reps
0.3
94.9
4.9
93.4
5.8
Adult Nutritional RTF High Protein, placebo
00821RF00
Total B1
3 days x 2 reps
0.4
97.7
4.3
95.4
5.5
Child Formula Powder, placebo
00847RF00
Total B1
3 days x 2 reps
1.0
99.1
5.7
97.0
7.0
Infant Elemantal Powder, placebo
00796RF
Total B1
3 days x 2 reps
0.1
93.7
6.4
92.4
7.8
Infant Formula Powder Partially Hydrolyzed Milk Based
410057652Z
Total B1
3 days x 2 reps
73.5
100.2
1.8
100.8
1.8
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z
Total B1
3 days x 2 reps
74.6
101.1
1.7
102.5
1.2
Infant Formula Powder Soy Based
E10NWZC
Total B1
3 days x 2 reps
98.6
98.7
0.7
94.5
1.5
Infant Formula RTF Milk Based, placebo
EV4H2Q
Total B1
3 days x 2 reps
3.3
96.9
4.3
95.6
6.1
MEAN
97.8
3.7
96.4
4.6
Adult Nutritional RTF High Fat, placebo
00820RF00
Total B2
3 days x 2 reps
48.7
97.2
1.6
95.6
1.7
Adult Nutritional RTF High Protein, placebo
00821RF00
Total B2
3 days x 2 reps
41.2
96.5
2.3
98.4
2.7
Child Formula Powder, placebo
00847RF00
Total B2
3 days x 2 reps
26.7
98.0
2.7
98.9
2.8
Infant Elemantal Powder, placebo
00796RF
Total B2
3 days x 2 reps
6.2
95.1
1.8
96.7
1.0
Infant Formula Powder Partially Hydrolyzed Milk Based
410057652Z
Total B2
3 days x 2 reps
159.0
99.9
1.8
99.7
2.4
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z
Total B2
3 days x 2 reps
101.0
100.2
2.0
99.6
1.9
Infant Formula Powder Soy Based
E10NWZC
Total B2
3 days x 2 reps
125.0
97.3
2.9
95.4
2.6
Infant Formula RTF Milk Based, placebo
EV4H2Q
Total B2
3 days x 2 reps
53.3
100.7
1.8
97.9
3.2
MEAN
98.1
2.1
97.8
2.3
Adult Nutritional RTF High Fat, placebo
00820RF00
Total B3
3 days x 2 reps
34.2
102.1
7.8
103.1
6.8
Adult Nutritional RTF High Protein, placebo
00821RF00
Total B3
3 days x 2 reps
24.4
101.7
5.9
102.9
3.8
Child Formula Powder, placebo
00847RF00
Total B3
3 days x 2 reps
10.4
105.4
6.3
105.7
5.3
Infant Elemantal Powder, placebo
00796RF
Total B3
3 days x 2 reps
5.7
104.5
6.8
103.8
4.9
Infant Formula Powder Partially Hydrolyzed Milk Based
410057652Z
Total B3
3 days x 2 reps
775.0
103.0
1.8
110.7
2.4
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z
Total B3
3 days x 2 reps
787.0
102.3
2.1
105.6
2.4
Infant Formula Powder Soy Based
E10NWZC
Total B3
3 days x 2 reps
843.0
101.8
1.6
100.3
3.3
Infant Formula RTF Milk Based, placebo
EV4H2Q
Total B3
3 days x 2 reps
23.2
105.3
5.8
103.4
7.0
MEAN
103.2
4.8
104.4
4.5
Adult Nutritional RTF High Fat, placebo
00820RF00
Total B6
3 days x 2 reps
4.6
100.2
3.2
99.5
2.7
Adult Nutritional RTF High Protein, placebo
00821RF00
Total B6
3 days x 2 reps
6.3
96.8
2.4
98.9
2.7
Child Formula Powder, placebo
00847RF00
Total B6
3 days x 2 reps
6.0
99.7
1.8
99.1
1.9
Infant Elemantal Powder, placebo
00796RF
Total B6
3 days x 2 reps
1.0
98.0
2.1
98.4
3.4
Infant Formula Powder Partially Hydrolyzed Milk Based
410057652Z
Total B6
3 days x 2 reps
54.4
99.1
1.3
100.1
2.4
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z
Total B6
3 days x 2 reps
56.1
100.1
2.5
100.5
2.6
Infant Formula Powder Soy Based
E10NWZC
Total B6
3 days x 2 reps
58.8
99.3
1.5
97.6
2.5
Infant Formula RTF Milk Based, placebo
EV4H2Q
Total B6
3 days x 2 reps
3.3
98.6
2.8
99.6
3.8
MEAN
99.0
2.2
99.2
2.8
Additional information to be completed by SD
yes
no
yes
yes
no
no
yes
yes
no
High (~200% Fort.)
Spike Recovery
Product
Nr. replicates (n)
Native level
ug/100g as RTF
Analyte
Low (~50% Fort.)
SPIFAN Code
Was a portion of the product spiked?
Were all spike recovery samples taken from the same spiked product?
Were multiple portions of the product spiked and each spiked product analyzed?
What percentage of the spiked sample was the spiked was the spike blanc? (How much was product diluted by spike?)
water
3% low-13% high
Mixed std
Were products spiked before they were weighed into extraction vessels?
Were all spike recovery samples prepared on multiple days?
Were spike recoveries calculated from theoretical additions?
Or was spiking solution analyzed and the results used to calculate spike recoveries?
Were all spike recovery samples prepared on the same day?
What form of the nutrient was spiked into the product?
What kind of solution or solvent was used to deliver the spike to the product?
Were products weighed into extraction vessels before spiking?
SPIFAN ERP Checklist v1.0
BVit-02 - MEF FORM
FOR ERP USE ONLY
DO NOT DISTRIBUTE