324 / 407
ERP SUMMARY FOR FIRST TO FINAL ACTION METHOD RECOMMENDATION
GUIDANCE FOR AOAC ERPS ‐ APPENDIX G
1
Considered?
Comments/Reference if applicable
Method Applicability
Yes
Meets SMPR
ERP First Action to Final Action
recommendations & improvements
Yes
Draft Final Action method reviewed by ERP Yes
Completed in June 2017
Safety Concerns
Yes
ReferenceMaterials
Yes
NIST 1849a and SPIFAN Materials
Single Laboratory Validation
Yes
Gill et al, Journal of AOAC Int 99, 5 (2016) p.1321
Reproducibility/Uncertaintyand
Probability of Detection
Yes
In publication pending review.
Comparison to SMPR (
SMPR criteria met?)
Yes
AOAC 2011.004
Feedback from Users of Method
Yes
All Addressed
DOCUMENTATION
Available?
Comments
Safety Evaluation
Yes
ReferenceMaterials
Yes
NIST 1849a and SPIFAN Materials
SLV or PTM
Yes
Gill et al, Journal of AOAC Int 99, 5 (2016) p.1321
Approved Validation Protocols
Yes
OMA Appendix L
Statistics Review
Method Published in OMA
Yes
Method Performance vs SMPR criteria
Yes
Meets the AOAC SMPR 2011.004
Feedback Information
Yes
All addressed
Additional Recognition(s)
Yes
Is a working item in ISO
ERP Reports
Yes
3‐16‐2016; 9‐20‐2016; 3‐16‐2017
Manuscript(s) Published in JAOAC
Yes
Gill et al, Journal of AOAC Int 99, 5 (2016) p.1321
(SLV); MLT publication in process
ERP Method Recommendation
(Final Action/Repeal/Continuation)
1
Official Methods of Analysis of AOAC INTERNATIONAL
, Appendix G: Procedures and Guidelines for the Use of AOAC Voluntary Consensus Standards
to Evaluate Characteristics of a Method of Analysis, p.3 “
First Action to Final Action Methods: Guidance for AOAC Expert Review Panels.”
AOAC 2016.05
Analysis of Vitamin D2 and Vitamin D3 by LC MS/MS in Milk Powders, Infant
Formulas, and Adult Nutritionals
216