347 / 407
Table 1 (continued). Tabulated raw data for replicate analyses of SPIFAN kit
Vitamin D
3
,
µg hg-
1
Vitamin D
2,
µg hg-
1
Lab #a
Milk-based child
Low-fat adult
formula powder
nutritional powder
CandidateSRM NIST 1869
(unfortified)
3
0.00
0.00
3.20
3.02
15.07
14.76
13.14
14.05
4
0.06
0.04
3.74
3.55
13.62
14.49
13.75
14.44
6
0.00
0.00
3.28
3.56
*21 09
*18.01
14.24
14.10
7
0.01
0.02
3.35
3.45
12.79
12.80
13.19
12.72
8
0.00
0.00
2.64
2.83
13 20
13.34
12.60
12.64
9
0.03
0.04
4.06
3.81
16.75
17.54
17.61
17.34
10
0.00
0.01
3.15
3.13
14.30
13.30
13.30
13.40
11
0.00
0.00
2.98
2.83
15.44
15.49
13.06
11.93
12
0.00
0.00
2.89
3.25
10.49
11.14
12.21
11.99
• Data for Labs 1, 2, and 5 not submitted prior to MLT submission deadline.
* Results removed as Cochran outlier prior to precision calculation.
23
2016.05 (VITAMIN D) FINAL ACTION REVIEW
FOR ERP USE ONLY
DO NOT DISTRIBUTE
239