Table1. Intermediateprecision results (mg/kg for thenineelementsof interest here) for 11SPIFAN
products (RSDs>5%highlighted). Analternate internal standard (Ni)was also tried for all
elements except Se.
Na
Mg
P
K
Ca
Cr*
Mn
Fe
Cu
Zn
Se*
Mo*
Adult NutritionRTF, HighFat - 00406RF00
Ni/Te
Overall mean (mg/kg)
1388.8
404.2
1029.0
2360.6
861.1
142.5
4.80
21.5
2.39
28.2
133.3
194.4
%RSD (N=8)
2.2
3.0
2.7
2.2
5.5
3.0
5.3
3.3
1.6
2.0
3.6
1.8
Overall mean (mg/kg)
1390.2
398.0
1006.7
2362.1
888.3
141.0
4.80
21.5
2.37
27.9
192.6
%RSD (N=8)
2.0
1.8
2.9
1.7
9.4
1.8
4.8
3.6
3.0
1.4
2.6
Adult NutritionRTF, HighProtein - 00414RF00
Ni/Te
Overall mean (mg/kg)
1022.4
324.5
936.3
1520.9
984.4
130.4
4.23
18.7
1.81
22.0
92.6
154.4
%RSD (N=8)
2.3
2.4
2.7
2.5
3.2
3.8
2.1
3.8
2.7
2.3
3.0
2.7
Overall mean (mg/kg)
1019.8
330.1
950.9
1564.6
982.9
129.9
4.22
18.7
1.81
22.0
154.1
%RSD (N=8)
1.9
3.4
3.4
3.9
2.8
2.9
2.1
3.4
3.0
2.4
3.2
Adult Nutr. PwdMilkProteinBased - 11750017V3
Ni/Te
Overall mean (mg/kg)
2243.6
424.8
2085.0
5736.4
2781.6
141.5
5.23
43.1
11.3
51.7
219.0
290.2
%RSD (N=8)
1.8
1.8
3.0
2.3
1.9
4.2
1.4
2.5
1.6
1.3
2.8
4.1
Overall mean (mg/kg)
2271.6
430.3
2135.6
5806.3
2816.8
142.5
5.30
43.8
11.5
52.4
293.7
%RSD (N=8)
2.2
3.3
2.4
1.7
2.3
5.0
2.6
4.0
3.3
2.6
4.9
Adult Nutritional Powder LowFat - 00394RF00
Ni/Te
Overall mean (mg/kg)
2030.1
1107.6
2621.7
4959.1
2688.7
419.6
13.7
58.5
6.21
60.8
267.6
552.3
%RSD (N=8)
2.9
2.4
3.3
2.3
2.2
1.3
1.7
2.3
2.2
1.7
3.2
1.9
Overall mean (mg/kg)
2072.1
1130.4
2706.8
5063.3
2745.2
428.2
14.0
59.8
6.34
62.1
564.6
%RSD (N=8)
2.8
2.9
1.8
2.1
2.7
1.3
2.7
3.5
3.3
2.6
3.0
ChildFormulaPowder - 00412RF00
Ni/Te
Overall mean (mg/kg)
1432.8
735.0
3416.4
5371.8
3716.2
268.8
7.46
56.5
5.04
36.8
213.0
255.4
%RSD (N=8)
2.8
3.7
2.4
2.6
2.4
1.9
1.8
2.6
4.2
1.5
2.9
4.8
Overall mean (mg/kg)
1456.4
741.4
3488.5
5497.1
3794.2
271.9
7.62
57.7
5.15
37.6
260.7
%RSD (N=8)
2.6
2.5
2.0
2.5
1.8
1.3
1.4
3.2
3.7
1.7
5.1
Infant Elemental Powder - 00403RF00
Ni/Te
Overall mean (mg/kg)
2369.9
478.2
4484.9
7813.5
6188.2
209.1
4.59
103.5
7.10
63.8
208.6
154.6
%RSD (N=8)
3.5
2.5
2.4
4.1
3.0
3.4
1.7
1.5
1.0
1.2
2.8
6.3
Overall mean (mg/kg)
2408.8
489.1
4559.6
7969.7
6305.4
215.3
4.67
104.8
7.20
64.6
160.0
%RSD (N=8)
3.0
3.3
2.4
3.1
2.2
6.3
1.3
1.9
1.7
2.1
7.5
Infant FormulaPowderMilkBased- D04HTCVV
Ni/Te
Overall mean (mg/kg)
1874.0
563.6
2802.9
6735.9
4692.8
47.1
1.05
116.7
5.45
65.9
230.5
161.8
%RSD (N=8)
3.2
3.2
2.1
3.2
3.0
8.5
2.5
1.4
3.9
1.4
3.8
6.5
Overall mean (mg/kg)
1867.8
564.9
2800.3
6747.9
4694.3
44.3
1.05
116.5
5.43
65.9
237.2
159.2
%RSD (N=8)
3.2
2.9
1.7
3.3
2.5
7.7
2.0
2.0
4.9
1.5
5.7
8.2
Infant FormPwdPartiallyHydrolyzedMilkBased - 1172572116
Ni/Te
Overall mean (mg/kg)
1554.4
377.0
2307.0
6417.1
4169.1
23.2
1.05
83.2
4.88
43.2
239.3
182.1
%RSD (N=8)
1.2
2.1
2.2
1.4
1.6
22.2
1.9
2.2
2.8
1.5
2.7
4.1
Overall mean (mg/kg)
1563.0
376.7
2308.2
6453.2
4193.1
21.4
1.05
83.7
4.90
43.4
183.8
%RSD (N=8)
1.8
2.6
4.4
1.1
2.2
20.2
2.6
3.1
3.9
2.6
4.0
Infant FormPwdPartiallyHydrolyzed soyBased - 117257651Z
Ni/Te
Overall mean (mg/kg)
2450.3
602.0
3930.6
7340.4
6428.0
55.1
2.29
109.7
4.84
48.8
241.5
296.1
%RSD (N=8)
2.3
2.4
3.1
1.7
1.6
8.8
2.1
1.5
3.2
1.5
4.1
2.8
Overall mean (mg/kg)
2470.1
604.5
3951.6
7399.9
6480.7
53.6
2.30
110.6
4.88
49.2
297.2
%RSD (N=8)
2.9
2.9
3.6
2.2
2.2
9.2
2.6
2.5
3.9
1.8
3.6
Infant FormulaRTFSoyBased- E29JVLV
Ni/Te
Overall mean (mg/kg)
2269.3
721.9
4283.9
7460.9
6500.5
72.4
3.28
112.9
5.36
73.1
223.2
320.2
%RSD (N=8)
1.8
2.8
2.5
2.7
1.4
3.8
1.4
1.8
2.7
1.9
3.3
4.4
Overall mean (mg/kg)
2301.3
726.4
4252.3
7540.0
6470.1
72.5
3.31
113.8
5.40
73.9
328.3
%RSD (N=8)
2.4
2.8
5.0
2.6
3.5
5.2
2.3
2.4
4.1
2.3
4.5
Infant FormulaRTF, MilkBased - SPIFANControl MilkForm
Ni/Te
Overall mean (mg/kg)
179.1
59.6
301.8
993.6
584.1
7.38
0.155
14.1
0.580
7.16
29.6
17.1
%RSD (N=8)
2.9
2.6
3.1
1.7
3.8
52.1
4.1
3.3
2.3
2.1
2.9
11.7
Overall mean (mg/kg)
178.5
59.4
298.3
1004.1
597.6
7.61
0.153
14.3
0.579
7.17
16.9
%RSD (N=8)
2.2
3.1
4.3
3.0
4.5
52.7
2.9
4.3
3.5
2.1
10.0
* Concentrations inng/g
Te - internal standardonly for Se
Ge
Ge
Ge
Ge
Ge
Ge
Ge
Ge
Ge
Ge
Ge
MTE-02
FORWORKINGGROUP/ERPUSEONLY
DONOTDISTRIBUTE
