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Table 3

Product

SPIFAN Code Analyte

Nr. replicates (n)

Conc. Level

RSDr

RSD iR

Conc. Level

RSDr

RSD iR

SRM 1849a

CLC10-B Tryptophan

12

20.1

0.4

1.5

X

≤ Z % ≤ W %

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z Tryptophan

12

25.3

0.6

1.0 Analyte 1

0.4-5.0

4%

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z Tryptophan

12

18.3

5.0

6.9 Analyte 2

Toddler Formula Powder Milk-Based

4052755861 Tryptophan

12

25.7

0.8

2.0 Analyte 3

Infant Formula Powder Milk-Based

4044755861 Tryptophan

12

24.1

0.2

1.8 Analyte 4

Adult Nutritional Powder Low Fat

00859RF00 Tryptophan

12

21.4

0.9

1.7 Analyte 5

Child Formula Powder

00866RF00 Tryptophan

12

23.7

0.9

1.3 Analyte 1

5.0-50

3%

Infant Elemental Powder

00795RF

Tryptophan

12

32.2

0.2

1.6 Analyte 2

Infant Formula Powder FOS/GOS Based

50350017W1 Tryptophan

12

23.2

2.0

2.4 Analyte 3

Infant Formula Powder Milk Based

K16NTAV Tryptophan

12

19.5

0.3

1.7 Analyte 4

Infant Formula Powder Soy Based

E10NWZC Tryptophan

12

18.3

0.2

2.3 Analyte 5

Infant Formula RTF Milk Based

EV4H2R

Tryptophan

12

22.4

0.5

1.8 Analyte 1

50-2500

2%

Adult Nutritional RTF High Prtotein

00730RF00 Tryptophan

12

70.6

1.9

3.7 Analyte 2

Adult Nutritional RTF High Fat

00729RF00 Tryptophan

12

91.3

0.3

1.9 Analyte 3

Analyte 4

Analyte 5

Analyte 1

Analyte 2

Analyte 3

Analyte 4

Analyte 5

Global Mean %

1.0

2.3

Precision - repeatability.

REQUIREMENTS SMPR

SPIFAN ERP X Checklist v 1.0

AMINO-02 (FEBRUARY 2017) - MEF FORM

FOR ERP USE ONLY

DO NOT DISTRIBUTE

24