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CAROT-03 (FEBRUARY 2017) - MEF FORM

FOR ERP USE ONLY

DO NOT DISTRIBUTE

Avg (%)

RSD % Avg (%) RSD (%)

Adult High Fat RTD

00729RF00

Lutein

6

6.65

95.3

5.4

Infant Soy Powder

E10NW2C

Lutein

6

2.45

93.9

4.4

Infant Hydrolyzed Milk Powder

410057652Z

Lutein

6

ND

Adult High Fat RTD

00729RF00

beta-carotene

6

0.26

108.1

6.9

Infant Soy Powder

E10NW2C

beta-carotene

6

17.5

89.3

6.5

Infant Hydrolyzed Milk Powder

410057652Z

beta-carotene

6

1.27

Adult High Fat RTD

00729RF00

Lycopene

6

ND

101.9

6.9

Infant Soy Powder

E10NW2C

Lycopene

6

ND

97.3

4.2

Infant Hydrolyzed Milk Powder

410057652Z

Lycopene

6

ND

ND= Not Detected

Global Mean % 101.8

6.4

93.5

5.0

Additional information to be completed by SD

yes

yes

no

no

yes

no

yes

no

yes

Analyte

trans lutein

Were all spike recovery samples prepared on multiple days?

Were spike recoveries calculated from theoretical additions?

Or was spiking solution analyzed and the results used to calculate spike recoveries?

Spike Level ~10 µg

SPIFAN Code

Was a portion of the product spiked?

Were all spike recovery samples taken from the same spiked product?

Were multiple portions of the product spiked and each spiked product analyzed?

Were products weighed into extraction vessels before spiking?

Were all spike recovery samples prepared on the same day?

Spike Level ~25 µg

Product

Nr. replicates (n)

Native level

Were products spiked before they were weighed into extraction vessels?

Spike Recovery

Spike Level ~10 µg Spike Level ~25 µg

Spike Level ~1 µg Spike Level ~2 µg

What form of the nutrient was spiked into the product?

What kind of solution or solvent was used to deliver the spike to the product?

What percentage of the spiked sample was the spiked was the spike blanc? (How much was product diluted by spike?)

Ethanol

1.5-7%

SPIFAN ERP Checklist v 1.0