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Day 1

2 311,5675077 155,7837538

4,2559746

Day 2

2

311,300509 155,6502545 0,104950096

Day 3

2 314,2306529 157,1153265 0,087835148

ANAVA

Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups

2,624895781

2 1,312447891 0,88504298 0,498761 9,552094

Within Groups

4,448759844

3 1,482919948

Total

7,073655625

5

Sl^2

-0,085236029

SR^2

1,397683919

Reproducibility (SR)

1,18 mg/kg

RSD%

0,8 %

Repeatability (Sr)

1,22 mg/kg

0,8 %

Sample name

Adult Nut. RFT High Fat

Sample nr.

487-2014-04020202

Rep 1 (mg/kg) Rep 2 (mg/kg)

Average of all days

Day 1

220,6765481 218,1061917

221,69 mg/kg

Day 2

220,4129711 223,8276604

Day 3

221,6249524 225,4660592

Anava: Single faktor

Summary

Groups

Count

Sum

Average

Variance

Day 1

2 438,7827398 219,3913699 3,303365957

Day 2

2 444,2406315 222,1203157 5,830051435

Day 3

2 447,0910115 223,5455058 7,377050819

ANAVA

Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups

17,82343769

2 8,911718846 1,619285183 0,333468 9,552094

Within Groups

16,51046821

3 5,503489404

Total

34,3339059

5

Sl^2

1,704114721

SR^2

7,207604125

Reproducibility (SR)

2,68 mg/kg

RSD%

1,2 %

Repeatability (Sr)

2,35 mg/kg

1,1 %

Free Carnitne:

Sample name

Lot#

Day 1

Day 2

Day 3

(mg/kg)

(mg/kg)

(mg/kg)

Child Formula Powder

00411RF00

Rep. 1

1,254160016 1,517589024

1,431514476

Child Formula Powder

00411RF00

Rep. 2

1,708356171 1,597505237

1,680537147

Infant Element Powder

00402RF00

Rep. 1

0,281750232 0,630450654

0,409483725

Infant Element Powder

00402RF00

Rep. 2

0,51285317 0,270410237

0,224943737

Adult Nut. RFT High Pro-

tein

00415RF00

Rep. 1

0,353030884 0,402888636

0,323884232

Adult Nut. RFT High Pro-

tein

00415RF00

Rep. 2

0,405091552 0,382089031

0,337483995

Adult Nut. RFT High Fat

00407RF00

Rep. 1

0,456936563 0,569845912

0,339190282

Adult Nut. RFT High Fat

00407RF00

Rep. 2

0,579822064 0,540715732

0,476087797

Infant Formula RFT, Milk

Based

Spifan Blank

Milk Form

Rep. 1

25,67551927 25,29927744

24,48829302

Carn-06 (Validation Report-Addendum)

FOR ERP USE ONLY

DO NOT DISTRIBUTE