230-231 / 427
SMPR Key Points: Identification Method
Parameter
Parameter Requirements
Target Test
Concentration
Minimum
Acceptable
Results
POI @ low
Minimum of 33 replicates
representing all target
compounds in Annex II and all
100 ppm
90% POI
§
of
the pooled
data for all
y Validation
concentration matrix types listed in Annex III,
spiked at or below the designated
low level target test conc.
target
compounds
and matrices
e Laborator
POI @ high
concentration
Minimum of 5 replicates per
matrix type spiked at 10x the
designated low level target test
10 x low conc.
100% correct
Singl
conc.
analyses are
expected
POI @ zero
concentration
Minimum of 5 replicates per
matrix type
0 ppm
.
§
95% confidence interval