92 / 427
6.
System suitability tests and/or analytical quality control:
80
Suitable methods will include blank check samples, and check standards at the lowest point
81
and midrange point of the analytical range.
82
83
7.
Potential
Reference Material(s):
84
85
Whole Egg
86
•
NIST 8445
87
•
LGC SAL-RSM-5 (Check for characterization level)
88
89
Nonfat Milk Powder
90
•
NIST SRM 1549 (nonfat milk powder)
91
•
NIST SRM 1549a (whole milk powder)
92
93
Peanut
94
•
NIST SRM 2387 (peanut butter)
95
•
LGC
FAL-RFM1017-XXX96
97
Hazelnut
98
•
No known reference material available.
99
•
LGC
FAL-RFM1015-50 or FAL-RFM1015-50Â o r FAL-RFM1015-5100
101
Additional materials can be found at the LGC and FAPAS websites
102
LGC
= http://www.lgcstandards.com/HK/en/search/?q=allergen:relevance:category:CEFP_77243103
FAPAS
= http://fapas.com/quality-control-materials/Available-quality-control-materials.cfm104
105
Refer to Annex F:
Development and Use of In-House Reference Materials
i
n Appendix F:106
Guidelines for Standard Method Performance Requirements
, 19
th
Edition of the AOAC
107
INTERNATIONAL Official Methods of Analysis (2012). Available at:
108
http://www.eoma.aoac.org/app_f.pdf109
110
NIST = National Institute for Standards and Technology.
111
LGC = formerly the UK
Laboratory of the Government Chemist
, now simply “LGC Standards”.
112
FAPAS = formerly the
Food Analysis Performance Assessment Scheme
in the UK, now simply
113
“FAPAS”.
114
115
116
8.
Validation Guidance
:
117
118
Method developers shall submit
LOQ, MDL, recovery and precision
data
evaluating for
the
119
matrices in Table 2.
120
121
Appendix D:Guidelines for Collaborative Study Procedures To Validate Characteristics of a
122
Method of Analysis; 19
th
Edition of the AOAC INTERNATIONAL Official Methods of Analysis
123
(2012). Available at:
http://www.eoma.aoac.org/app_d.pdf124
125
Appendix F:Guidelines for Standard Method Performance Requirements; 19
th
Edition of the
126
AOAC INTERNATIONAL Official Methods of Analysis (2012). Available at:
127
http://www.eoma.aoac.org/app_f.pdf128
129
9.
Maximum Time-To-Result:
None
130
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