5 / 5
93
Table 2: Method performance requirements (part 1).
94
Parameter
Requirement
THC, THCA, CBDA, CBD, Individually
Reported
Requirement (Additional, Desirable
Cannabinoids (Table 1b), including
CBN)
Limit of Quantitation (LOQ) (% w/w)
≤ 0.3
≤ 0.3
Analytical Range (% w/w)
≤ 0.3 – ca. 100
≤ 0.3 – ca. 50
*Reported as individual cannabinoids
95
96
97
98
99
100
101
102
103
104
105
106
Table 3: Method performance requirements (part 2).
Parameters
Ranges (% w/w)
≤ 0.3 – 1
> 1 ‐ 10
> 10 – ca. 100
Recovery (% w/w)
95 – 105
97 ‐ 103
98 ‐ 102
% RSD
r
≤ 5
≤ 4
≤ 2
% RSD
R
≤ 7
≤ 5
≤ 3