AOAC SPIFAN Nutrients ERP (April 26, 2017) Virtual Meeting

152-153 / 154

All results for both SPIFAN and IDF samples. Results in orange were omited from the statistics.
AdultNutritionalPowder LowFat AdultNutritionalRTFHighFat (liq.) Toddler FormulaPowderMilk-Based Child formulapowder–milk-basedplacebo
Lab LYNY751 PZGP859 Lab DYLB360 ZMQM883 Lab IQVG111 VVOL664 Lab DOMY545 FPTE312 Lab YMZB323 BYJK962 Lab EFXN778 BFAO941 Lab YXBH789 DRWO880
1 386.25 385.07 1 163.31 163.91 1 36.96 36.87 1 152.58 154.97 1 40.43 36.86 1 470.91 486.86 1 29.40 31.91
2 387.91 386.32 2 170.69 167.93 2 41.30 39.24 2 162.54 159.15 2 38.81 37.52 2 475.83 470.29 2 19.54 20.56
3 383.56 388.76 3 162.26 165.36 3 98.32 93.68 3 151.17 152.91 3 94.75 99.75 3 480.80 493.48 3 30.75 66.77
4 388.51 386.66 4 156.64 158.64 4 31.09 31.43 4 152.55 152.77 4 37.75 37.77 4 471.99 470.81 4 25.09 25.04
5 396.67 393.25 5 167.23 167.26 5 37.29 34.25 5 158.69 157.11 5 40.68 40.08 5 489.55 491.87 5 36.14 36.72
6 382.55 385.32 6 105.80 102.71 6 23.35 22.11 6 152.96 152.57 6 30.11 29.85 6 477.12 480.13 6 37.80 35.45
7 381.93 380.74 7 155.51 158.13 7 38.46 39.06 7 153.46 155.41 7 42.37 41.89 7 475.77 475.66 7 35.47 34.91
8 386.68 389.36 8 158.59 125.02 8 33.97 30.80 8 155.77 155.39 8 39.97 39.99 8 479.53 480.51 8 130.73 126.45
9 383.10 382.53 9 65.49 73.26 9 28.32 33.94 9 152.59 152.05 9 40.19 39.61 9 470.22 474.63 9 37.08 34.26
10 385.96 385.31 10 141.95 10 82.57 10 147.54 152.23 10 38.95 38.08 10 483.47 480.42 10 54.15 27.23
11 383.72 383.95 11 162.01 165.16 11 33.98 32.38 11 155.80 155.64 11 40.84 40.65 11 474.61 477.15 11 34.85 21.15
12 416.29 408.48 12 157.35 161.12 12 39.66 44.65 12 160.54 163.56 12 49.95 47.61 12 515.86 512.39 12 74.11 288.80
13 380.19 380.18 13 162.73 160.65 13 36.04 36.01 13 153.34 153.66 13 41.69 40.82 13 476.08 474.73 13 35.92 34.22
14 345.39 343.88 14 164.03 163.10 14 36.22 38.30 14 154.03 154.25 14 41.17 40.99 14 423.49 426.57 14 28.48 35.27
15 390.06 393.01 15 107.56 120.14 15 33.19 34.96 15 155.26 155.37 15 42.04 42.57 15 486.57 490.19 15 63.05 62.72
16 394.61 389.48 16 128.30 51.15 16 32.19 23.15 16 151.71 136.65 16 41.73 49.90 16 491.39 486.69 16 46.59 36.90
Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 10.00 Totalnumberof laboratories p 8.00 Totalnumberof laboratories p 16 Totalnumberof laboratories p 11.00 Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 11
Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 20.00 Totalnumberof replicates Sum(n(L)) 16.00 Totalnumberof replicates Sum(n(L)) 32 Totalnumberof replicates Sum(n(L)) 22.00 Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 22
Overallmeanofalldata (grandmean) XBARBAR 385.49 Overallmeanofalldata (grandmean) XBARBAR 162.65 Overallmeanofalldata (grandmean) XBARBAR 35.41 Overallmeanofalldata (grandmean) XBARBAR 154.19 Overallmeanofalldata (grandmean) XBARBAR 40.20 Overallmeanofalldata (grandmean) XBARBAR 478.61 Overallmeanofalldata (grandmean) XBARBAR 32.40
Repeatability standarddeviation s(r) 2.25 Repeatability standarddeviation s(r) 1.70 Repeatability standarddeviation s(r) 1.11 Repeatability standarddeviation s(r) 2.99 Repeatability standarddeviation s(r) 0.45 Repeatability standarddeviation s(r) 4.17 Repeatability standarddeviation s(r) 4.00
Reproducibility standarddeviation s(R) 13.34 Reproducibility standarddeviation s(R) 4.14 Reproducibility standarddeviation s(R) 2.55 Reproducibility standarddeviation s(R) 4.65 Reproducibility standarddeviation s(R) 1.56 Reproducibility standarddeviation s(R) 17.97 Reproducibility standarddeviation s(R) 6.75
Repeatability relative standarddeviation RSD(r) 0.58 Repeatability relative standarddeviation RSD(r) 1.05 Repeatability relative standarddeviation RSD(r) 3.14 Repeatability relative standarddeviation RSD(r) 1.94 Repeatability relative standarddeviation RSD(r) 1.12 Repeatability relative standarddeviation RSD(r) 0.87 Repeatability relative standarddeviation RSD(r) 12.35
Reproducibility relative standarddeviation RSD(R) 3.46 Reproducibility relative standarddeviation RSD(R) 2.54 Reproducibility relative standarddeviation RSD(R) 7.21 Reproducibility relative standarddeviation RSD(R) 3.01 Reproducibility relative standarddeviation RSD(R) 3.89 Reproducibility relative standarddeviation RSD(R) 3.76 Reproducibility relative standarddeviation RSD(R) 20.84
HORRATvalue 0.75 HORRATvalue 0.48 HORRATvalue 1.09 HORRATvalue 0.57 HORRATvalue 0.60 HORRATvalue 0.84 HORRATvalue 3.11
InfantFormulaRTFMilkBased (liq.) InfantFormulaPowder SoyBased InfantFormulaPowderMilkBased InfantFormulaPowder FOS/GOSBased
Lab XKIP216 HYJU890 Lab TJHR217 OACN211 Lab CULF358 GBZC169 Lab WKHN288 URTF231 Lab SWUO667 MYHK654 Lab KDOX966 ATAN351
1 42.06 42.69 1 501.01 507.10 1 407.92 415.97 1 336.36 325.69 1 384.34 395.03 1 384.52 386.45
2 43.66 41.99 2 525.42 516.52 2 402.60 404.55 2 329.51 324.40 2 391.95 392.28 2 392.43 392.64
3 94.84 99.28 3 498.04 524.53 3 421.27 409.17 3 332.26 318.47 3 390.17 391.08 3 382.22 385.47
4 42.10 42.22 4 507.78 507.19 4 404.98 408.86 4 325.94 320.87 4 387.74 385.88 4 376.98 380.89
5 42.75 42.79 5 516.52 518.37 5 417.37 416.50 5 335.20 336.88 5 393.92 395.87 5 382.32 383.20
6 41.90 41.96 6 505.70 506.16 6 407.97 406.92 6 327.43 328.39 6 383.76 382.43 6 375.71 375.62
7 41.78 41.86 7 503.84 504.06 7 405.95 405.71 7 325.64 327.40 7 380.68 381.54 7 374.60 373.61
8 42.28 42.16 8 508.50 507.65 8 410.15 409.71 8 331.26 329.92 8 385.33 386.07 8 376.65 375.79
9 41.26 41.37 9 497.93 499.74 9 401.03 402.16 9 324.05 325.28 9 379.06 376.15 9 371.58 369.11
10 42.09 42.18 10 409.25 506.83 10 409.47 409.47 10 327.90 329.14 10 382.63 383.84 10 375.61 376.37
11 41.03 42.08 11 503.83 503.25 11 405.97 407.00 11 326.04 325.91 11 381.44 383.05 11 374.00 417.45
12 45.14 45.59 12 530.45 538.07 12 445.84 464.35 12 358.55 353.14 12 417.15 418.94 12 393.84 402.15
13 41.81 42.19 13 500.94 500.72 13 404.77 405.31 13 325.26 325.18 13 378.98 379.34 13 370.86 370.54
14 41.86 41.83 14 436.23 503.87 14 330.72 363.97 14 293.67 394.11 14 340.64 347.08 14 371.89 370.30
15 43.10 42.95 15 516.86 515.43 15 414.27 440.22 15 332.24 335.65 15 407.10 399.49 15 390.73 384.22
16 42.67 42.62 16 508.55 513.10 16 413.72 432.16 16 334.08 332.98 16 383.14 132.46 16 280.34 379.96
Total numberof laboratories p 15 Totalnumberof laboratories p 14 Totalnumberof laboratories p 15 Totalnumberof laboratories p 15 Totalnumberof laboratories p 15 Total numberof laboratories p 14
Total numberof replicates Sum(n(L)) 30 Totalnumberof replicates Sum(n(L)) 28 Totalnumberof replicates Sum(n(L)) 30 Totalnumberof replicates Sum(n(L)) 30 Totalnumberof replicates Sum(n(L)) 30 Total numberof replicates Sum(n(L)) 28
Overallmean ofall data (grand mean) XBARBAR 42.40 Overallmeanofalldata (grandmean) XBARBAR 510.26 Overallmeanofalldata (grandmean) XBARBAR 413.71 Overallmeanofalldata (grandmean) XBARBAR 330.37 Overallmeanofalldata (grandmean) XBARBAR 386.10 Overallmean ofall data (grand mean) XBARBAR 380.22
Repeatability standard deviation s(r) 0.40 Repeatability standarddeviation s(r) 5.69 Repeatability standarddeviation s(r) 7.28 Repeatability standarddeviation s(r) 3.70 Repeatability standarddeviation s(r) 2.83 Repeatability standard deviation s(r) 2.34
Reproducibility standard deviation s(R) 0.99 Reproducibility standarddeviation s(R) 10.24 Reproducibility standarddeviation s(R) 14.45 Reproducibility standarddeviation s(R) 8.40 Reproducibility standarddeviation s(R) 15.77 Reproducibility standard deviation s(R) 8.63
Repeatability relative standard deviation RSD(r) 0.94 Repeatability relative standarddeviation RSD(r) 1.12 Repeatability relative standarddeviation RSD(r) 1.76 Repeatability relative standarddeviation RSD(r) 1.12 Repeatability relative standarddeviation RSD(r) 0.73 Repeatability relative standard deviation RSD(r) 0.61
Reproducibility relative standard deviation RSD(R) 2.34 Reproducibility relative standarddeviation RSD(R) 2.01 Reproducibility relative standarddeviation RSD(R) 3.49 Reproducibility relative standarddeviation RSD(R) 2.54 Reproducibility relative standarddeviation RSD(R) 4.08 Reproducibility relative standard deviation RSD(R) 2.27
HORRATvalue 0.36 HORRATvalue 0.45 HORRATvalue 0.76 HORRATvalue 0.54 HORRATvalue 0.88 HORRATvalue 0.49
InfantFormulaPowderMilkBased Child formulapowder–milk-based SRM1849a Infantelementalpowderplacebo InfantElemantalPowder
Lab TJMN542 XJDD334 Lab JSDT587 NSRB999 Lab RQXQ518 GVPE615 Lab KGSZ273 LTCT316 Lab ARJT349 SAEQ748 Lab UOPM297 ECHL425
1 22.57 23.47 1 363.09 364.96 1 439.04 437.77 1 697.62 693.35 1 369.61 364.11 1 383.06 387.06
2 22.38 21.97 2 361.11 360.12 2 441.29 448.32 2 715.80 706.81 2 368.05 365.69 2 384.18 382.42
3 23.44 22.00 3 368.43 361.66 3 442.32 442.91 3 736.73 748.59 3 366.09 363.13 3 382.07 377.58
4 22.43 22.52 4 357.30 359.79 4 435.77 437.91 4 694.07 688.54 4 360.00 360.03 4 378.65 378.60
5 22.47 22.53 5 366.56 367.73 5 452.74 453.54 5 704.76 706.44 5 361.34 363.55 5 379.50 377.76
6 22.16 21.93 6 357.90 359.40 6 444.88 442.87 6 693.23 696.90 6 354.09 355.34 6 371.79 370.09
7 21.90 22.18 7 354.18 357.11 7 435.71 438.29 7 696.55 694.88 7 353.17 352.11 7 368.40 369.51
8 22.21 22.35 8 360.64 360.09 8 447.04 448.06 8 676.90 694.77 8 354.51 354.16 8 371.88 369.74
9 21.88 21.90 9 471.79 476.13 9 444.46 442.87 9 692.68 692.24 9 352.24 351.69 9 368.49 367.62
10 22.34 21.83 10 360.50 359.06 10 446.14 447.87 10 685.88 695.90 10 353.37 354.27 10 370.44 370.62
11 21.95 22.00 11 356.40 357.15 11 441.76 442.52 11 687.18 687.19 11 352.69 353.18 11 368.80 368.69
12 24.53 24.54 12 510.02 505.38 12 475.80 472.78 12 736.99 736.42 12 377.11 383.63 12 394.06 393.72
13 22.05 21.80 13 355.16 356.56 13 440.75 440.28 13 687.75 688.02 13 349.77 350.91 13 365.75 368.94
14 22.09 22.03 14 308.39 324.36 14 395.93 397.62 14 695.72 688.33 14 353.18 353.24 14 318.73 334.04
15 23.91 23.85 15 490.10 487.76 15 462.68 459.76 15 705.69 709.07 15 362.35 360.57 15 377.96 376.66
16 22.02 22.15 16 365.89 365.48 16 450.81 445.53 16 697.10 702.45 16 354.54 358.13 16 373.47 371.15
Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 13.00 Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 16.00 Totalnumberof laboratories p 16
Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 26.00 Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 32.00 Totalnumberof replicates Sum(n(L)) 32
Overallmeanofalldata (grandmean) XBARBAR 22.48 Overallmeanofalldata (grandmean) XBARBAR 357.27 Overallmeanofalldata (grandmean) XBARBAR 443.63 Overallmeanofalldata (grandmean) XBARBAR 701.08 Overallmeanofalldata (grandmean) XBARBAR 358.93 Overallmeanofalldata (grandmean) XBARBAR 372.54
Repeatability standarddeviation s(r) 0.33 Repeatability standarddeviation s(r) 3.56 Repeatability standarddeviation s(r) 1.96 Repeatability standarddeviation s(r) 5.01 Repeatability standarddeviation s(r) 1.88 Repeatability standarddeviation s(r) 3.08
Reproducibility standarddeviation s(R) 0.79 Reproducibility standarddeviation s(R) 13.10 Reproducibility standarddeviation s(R) 15.80 Reproducibility standarddeviation s(R) 17.14 Reproducibility standarddeviation s(R) 8.03 Reproducibility standarddeviation s(R) 14.52
Repeatability relative standarddeviation RSD(r) 1.49 Repeatability relative standarddeviation RSD(r) 1.00 Repeatability relative standarddeviation RSD(r) 0.44 Repeatability relative standarddeviation RSD(r) 0.72 Repeatability relative standarddeviation RSD(r) 0.52 Repeatability relative standarddeviation RSD(r) 0.83
Reproducibility relative standarddeviation RSD(R) 3.50 Reproducibility relative standarddeviation RSD(R) 3.67 Reproducibility relative standarddeviation RSD(R) 3.56 Reproducibility relative standarddeviation RSD(R) 2.44 Reproducibility relative standarddeviation RSD(R) 2.24 Reproducibility relative standarddeviation RSD(R) 3.90
HORRATvalue 0.49 HORRATvalue 0.78 HORRATvalue 0.79 HORRATvalue 0.58 HORRATvalue 0.48 HORRATvalue 0.84
IDF samples
Butter
Lab IDF51** IDF71** Lab IDF106* IDF86* Lab IDF34 IDF94 Lab IDF23 IDF123 Lab IDF12 IDF42 Lab IDF65 IDF115
1 1 1 1 1 1
2 2 2 2 2 2
3 3 3 3 3 3
4 4 4 4 4 4
5 376.68 375.80 5 563.87 555.39 5 169.94 170.82 5 712.56 719.99 5 95.79 94.31 5 285.73 283.26
6 406.92 403.94 6 568.91 571.36 6 164.12 167.80 6 711.98 712.20 6 93.24 93.57 6 280.15 277.38
7 363.72 368.53 7 541.13 540.22 7 166.48 164.63 7 714.92 714.10 7 113.46 95.20 7 1533.24 1528.70
8 360.44 370.78 8 554.96 560.68 8 167.21 170.30 8 705.27 704.79 8 94.86 94.02 8 278.01 276.85
9 364.42 369.26 9 547.67 561.02 9 163.98 156.73 9 694.81 702.11 9 93.62 93.16 9 1561.30 1459.20
10 371.31 378.02 10 533.74 555.76 10 174.12 171.05 10 709.42 712.77 10 94.95 95.19 10 277.72 278.77
11 365.12 364.13 11 562.23 561.41 11 163.52 163.57 11 702.28 696.09 11 95.01 95.03 11 1510.67 1448.95
12 391.69 393.21 12 587.67 577.30 12 216.98 210.99 12 768.06 752.91 12 99.53 101.52 12 307.35 303.13
13 377.14 360.18 13 549.69 572.47 13 163.81 166.12 13 696.29 697.04 13 94.18 94.75 13 270.25 274.02
14 374.29 382.31 14 590.45 589.27 14 171.01 175.80 14 713.88 712.48 14 14 275.32 274.29
15 368.72 384.94 15 566.80 579.23 15 183.77 185.84 15 733.17 729.46 15 97.79 97.74 15 287.31 283.30
16 19.22 29.03 16 69.89 38.93 16 147.91 162.93 16 691.92 690.72 16 97.77 96.66 16 273.20 622.36
17 375.87 364.50 17 557.43 545.02 17 167.71 162.69 17 701.81 699.88 17 94.386 89.05 17 275.66 275.08
Totalnumberof laboratories p 12 Totalnumberof laboratories p 12 Totalnumberof laboratories p 10 Totalnumberof laboratories p 13 Totalnumberof laboratories p 11 Totalnumberof laboratories p 9
Totalnumberof replicates Sum(n(L)) 24 Totalnumberof replicates Sum(n(L)) 24 Totalnumberof replicates Sum(n(L)) 20 Totalnumberof replicates Sum(n(L)) 26 Totalnumberof replicates Sum(n(L)) 22 Totalnumberof replicates Sum(n(L)) 18
Overallmeanofalldata (grandmean) XBARBAR 375.50 Overallmeanofalldata (grandmean) XBARBAR 562.24 Overallmeanofalldata (grandmean) XBARBAR 169.52 Overallmeanofalldata (grandmean) XBARBAR 711.57 Overallmeanofalldata (grandmean) XBARBAR 95.28 Overallmeanofalldata (grandmean) XBARBAR 281.31
Repeatability standarddeviation s(r) 6.31 Repeatability standarddeviation s(r) 8.45 Repeatability standarddeviation s(r) 2.17 Repeatability standarddeviation s(r) 3.97 Repeatability standarddeviation s(r) 1.30 Repeatability standarddeviation s(r) 1.91
Reproducibility standarddeviation s(R) 13.03 Reproducibility standarddeviation s(R) 15.74 Reproducibility standarddeviation s(R) 6.53 Reproducibility standarddeviation s(R) 18.32 Reproducibility standarddeviation s(R) 2.59 Reproducibility standarddeviation s(R) 10.04
Repeatability relative standarddeviation RSD(r) 1.68 Repeatability relative standarddeviation RSD(r) 1.50 Repeatability relative standarddeviation RSD(r) 1.28 Repeatability relative standarddeviation RSD(r) 0.56 Repeatability relative standarddeviation RSD(r) 1.37 Repeatability relative standarddeviation RSD(r) 0.68
Reproducibility relative standarddeviation RSD(R) 3.47 Reproducibility relative standarddeviation RSD(R) 2.80 Reproducibility relative standarddeviation RSD(R) 3.85 Reproducibility relative standarddeviation RSD(R) 2.57 Reproducibility relative standarddeviation RSD(R) 2.72 Reproducibility relative standarddeviation RSD(R) 3.57
HORRATvalue 0.75 HORRATvalue 0.64 HORRATvalue 0.74 HORRATvalue 0.61 HORRATvalue 0.48 HORRATvalue 0.74
InfantFormulaRTF,MilkBased (liq.)PLACEBO
Adultnutritional ready to feed–high fatplacebo AdultNutritionalRTFHighProtein (liq.) Adultnutritional ready to feed–highproteinplacebo
InfantFormulaPowderPartiallyHydrolyzedSoyBased InfantFormulaPowderPartiallyHydrolyzedMilkBased
Processed cheese Wheyprotein concentrate Wholemilkpowder WholeMilk,1.0gas is Wheypowder
2016.03 (APRIL 2017) - MTE-01/03
MLT RESULTS
FOR ERP USE ONLY
DO NOT DISTRIBUTE