96 / 129
Table 3. Precision data for Milk-based IF
Day 1
Day 2
Day 3
Day 4
Day 5
Day 6
% RSD
PYR
3862
3685
3500
3642
3699
3946
3869
3695
3494
3679
3690
3916
4038
3676
3653
3760
3633
3752
PAL
569
559
552
560
560
565
580
590
573
594
567
629
551
576
591
591
563
592
PAM
216
99
105
112
112
107
210
99
80
116
117
110
206
90
112
113
110
107
Total
B
6
Average
4701
4358
4221
4390
4351
4576
3.4
THI
11622
11830
11459
11310
11666
11833
1.4
11741
11540
11415
11910
11319
11899
11896
11747
11619
11838
11263
11882
Total
THI
Average
11753
11706
11498
11686
11416
11871
RIB
11082
11119
10681
11371
11425
10894
2.2
10970
11361
10739
11224
11061
11008
11065
11272
10681
11367
11383
10961
Total
RIB
Average
11039
11251
10700
11321
11290
10954
Table 4. Spike recoveries of Non-phosphorylated Vitamins in Placebo product.
Day 1
Day 2
Day 3
Average
Spike Level
1
Pyr
107.3
98.7
89.3
98.5
Pal
102.2
100
106.5
102.9
Pam
102.2
98.6
100
100.3
Thi
100.4
98.4
98.8
99.2
Rib
98.5
99.3
99.8
99.2
Spike Level
2
Pyr
94.7
93.1
98.4
95.4
Pal
101.9
100.3
103.6
101.9
Pam
103.8
105.6
103.8
104.4
Thi
100.4
102.1
99.6
100.7
Rib
97.9
100
100.8
99.6
13
BVIT-02
FOR ERP/WORKING GROUP USE ONLY
DO NOT DISTRIBUTE