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93

Table 2: Method performance requirements (part 1).

94

Parameter

Requirement

THC, THCA, CBDA, CBD, Individually

Reported

Requirement (Additional, Desirable

Cannabinoids (Table 1b), including

CBN)

Limit of Quantitation (LOQ) (% w/w)

≤ 0.3

≤ 0.3

Analytical Range (% w/w)

0.3 – ca. 100

0.3 – ca. 50

*Reported as individual cannabinoids

95

96

97

98

99

100

101

102

103

104

105

106

Table 3: Method performance requirements (part 2).

Parameters

Ranges (% w/w)

0.3 – 1

> 1 - 10

> 10 – ca. 100

Recovery (% w/w)

95 – 105

97 - 103

98 - 102

% RSD

r

≤ 5

≤ 4

≤ 2

% RSD

R

≤ 7

≤ 5

≤ 3