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Analytical Range and LOQ Requirements

Total Glycosides

Analytical Range:

10– 250,000 ppm

Limit of Quantitation ≤10 ppm

Aglycones

Analytical Range:

10 – 20,000 ppm

Limit of Quantitation ≤10 ppm

Range, ppm

10‐100 >100 – 1,000 1,000 – 10,000 >10,000

Recovery, Repeatability, and Recovery for

both Total Glycosides and Aglycones

Recovery,  %

80‐110

90 – 107

95 – 105

97 – 103

Repeatability, %

≤ 7

≤ 6

≤ 4

≤ 1

Reproducibility, % ≤ 10

≤ 9

≤ 6

≤ 2