64 / 172
49
4.
Method Performance Requirements
:
50
See Table III
51
52
5.
System suitability tests and/or analytical quality control:
53
Methods will include a protocol to demonstrate sensitivity and specificity.
54
55
6.
Reference Material(s):
56
Refer t
o Annex F:Development and Use of In-House Reference Materials
in Appendix F:
57
Guidelines for Standard Method Performance Requirements
℠, 19
th
Edition of the AOAC
58
INTERNATIONAL
Official Methods of Analysis
(2012).
59
60
Selection of authentic materials from vouchered and/or accredited sources
61
62
Hildreth, J. et al. (2007)
Anal. Bioanal. Chem
.
389
, 13–17
63
64
Applequist, W., & Miller (2013)
Anal. Bioanal. Chem
.
405
, 4419–4428
65
66
National Center for Natural Products Research, University of Mississippi, Oxford, MS
67
68