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2.

Does the method contain system suitability tests or controls as specified by the SMPR? If no,

please indicate if there is a need for such tests or controls and which ones.

Yes.

3.

Is there information demonstrating that the method system suitability tests and controls as

specified in the SMPR worked appropriately and as expected? If no, please specify.

Yes, they could have demonstrated a broader range of standards.

4.

Based on the supporting information, is the method written clearly and concisely? If no, please

specify the needed revisions.

Yes, well written and easily followed.

5.

Based on the supporting information, what are pros/strengths of the method?

Method illustrates applicability of=ver wa wide range of test materials and includes clean up

procedures to remove interferences.

6.

Based on the supporting information, what are cons/weaknesses of the method?

Method is clearly described, would be useful in a range of materials and allows a range of test

procedures form single reagent or dual reagent to microplate.

7.

Any general comments about the method?

Method is useful over a broad range of testing. Better description of appropriate standards

would be beneficial.

V.

RECOMMENDATION FOR THE METHOD:

1.

Do you recommend this method be adopted as a First Action and published in the

Official

Methods of Analysis of AOAC INTERNATIONAL?

If no, please specify rationale.

Yes.