Laboratory & Quality Services
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van
8
Overview
Table 7. Overview performances
Analyte
Mn
Cu
Fe
Zn
Mg
P
Na
Ca
K
Lower analytical
range
a
0,003
0,010
0,2
0,01
0,09
0,04
0,5
0,4
6
Upper analytical
range
b
5
5
125
25
375
1250
625
1875
1875
Limit of
Quantitation
(LOQ)
0,003
0,010
0,2
0,01
0,09
0,04
0,5
0,4
6
Repeatibility ≤
(RSD)
c
1,2%
0,5%
1,3%
1,8%
1,5%
1,0%
0,7%
1,7%
0,8%
Recovery
d
97,4%
100,3%
96,9% 96,0% 97,6%
103,7%
95,5%
98,9%
98,5%
Reproducibility ≤
(RSD)
e
1,4%
1,7%
0,9%
1,0%
1,2%
1,0%
1,2%
1,2%
1,4%
a
Lower analytical range is equivalent to the LOQ.
b
Upper analytical range is equivalent to the highest standard (5) of the calibration curve used on daily
basis calculated by multiplying this standard by a dilution factor of 25.
c
Repeatibility of NIST SRM 1849a calculated by using the residues of the duplicates on 9 different days.
d
Overall average for 3 independent days using NIST SRM 1849a and the laboratory control sample
CM01/07.
e
Reproducibility of NIST SRM 1849a calculated by using the average results of the duplicates on 9
different days.
*mg/100g reconstituted final product.
MTE-03-SLV
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