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Table 3

Product

SPIFAN Code

Analyte

Nr. replicates (n) Conc. Level

RSDr

RSD iR

Conc. Level

RSDr

RSD iR

Child Formula Powder

00411RF00

Total Carnetine

6 0.24 mg/100 g

9.3

X

≤ Z % ≤ W %

Infant Element Powder

00402RF00

Total Carnetine

6 0.02 mg/100 g

48.5

Carnitine

Adult Nut. RFT High Protein

00415RF00

Total Carnetine

6 0.04 mg/100 g

19.3

Analyte 2

Adult Nut. RFT High Fat

00407RF00

Total Carnetine

6 0.05 mg/100 g

7.5

Analyte 3

Infant Formula RFT, Milk Based Spifan Blank Milk Form Total Carnetine

6 2.69 mg/100 g

2.6

Analyte 4

SRM 1849a

CLC10-b

Total Carnetine

6 15.18 mg/100 g

1.8

Analyte 5

Adult Nut. Protein Based

11750017V3

Total Carnetine

6 0.09 mg/100 g

26.9

Analyte 1

Infant Formula, Part. Hyd. Milk

1172572116 Total Carnetine

6 10.53 mg/100 g

2.5

Analyte 2

Infant Formula, Part. Hyd. Soy 117257651Z

Total Carnetine

6 9.33 mg/100 g

1.4

Analyte 3

Adult Nut. Low Fat

00394RF00

Total Carnetine

6 0.33 mg/100 g

12.8

Analyte 4

Child Formula

000412RF00

Total Carnetine

6 49.05 mg/100 g

1.0

Analyte 5

Infant Elemental

000403RF00

Total Carnetine

6 13.74 mg/100 g

1.0

Analyte 1

Infant Formula, Milk Based

D04HTCVV

Total Carnetine

6 15.91 mg/100 g

1.7

Analyte 2

Infant Formula, Soy Based

E29JVLV

Total Carnetine

6 8.28 mg/100 g

4.5

Analyte 3

Infant Formula RFT, Milk Based Spifan Control Milk Form Total Carnetine

6 2.79 mg/100 g

1.3

Analyte 4

Adult Nut. RFT High Protein

000414RF00

Total Carnetine

6 15.62 mg/100 g

0.8

Analyte 5

Adult Nut. RFT High Fat

00406RF00

Total Carnetine

6 22.17 mg/100 g

1.1

Analyte 1

Child Formula Powder

00411RF00

Free Carnetine

6 0.15 mg/100 g

14.0

Analyte 2

Infant Element Powder

00402RF00

Free Carnetine

6 0.04 mg/100 g

49.0

Analyte 3

Adult Nut. RFT High Protein

00415RF00

Free Carnetine

6 0.04 mg/100 g

6.4

Analyte 4

Adult Nut. RFT High Fat

00407RF00

Free Carnetine

6 0.05 mg/100 g

15.4

Analyte 5

Infant Formula RFT, Milk Based Spifan Blank Milk Form Free Carnetine

6 2.51 mg/100 g

1.8

SRM 1849a

CLC10-b

Free Carnetine

6 13.08 mg/100 g

2.9

Adult Nut. Protein Based

11750017V3

Free Carnetine

6 0.07 mg/100 g

15.5

Infant Formula, Part. Hyd. Milk

1172572116 Free Carnetine

6 8.19 mg/100 g

3.6

Infant Formula, Part. Hyd. Soy 117257651Z

Free Carnetine

6 9.18 mg/100 g

3.0

Adult Nut. Low Fat

00394RF00

Free Carnetine

6 0.21 mg/100 g

4.0

Child Formula

000412RF00

Free Carnetine

6 48.45 mg/100 g

0.7

Infant Elemental

000403RF00

Free Carnetine

6 13.57 mg/100 g

1.5

Infant Formula, Milk Based

D04HTCVV

Free Carnetine

6 13.85 mg/100 g

1.4

Infant Formula, Soy Based

E29JVLV

Free Carnetine

6 8.16 mg/100 g

1.3

Infant Formula RFT, Milk Based Spifan Control Milk Form Free Carnetine

6 2.60 mg/100 g

1.0

Adult Nut. RFT High Protein

000414RF00

Free Carnetine

6 15.26 mg/100 g

0.2

Adult Nut. RFT High Fat

00406RF00

Free Carnetine

6 21.67 mg/100 g

3.0

Global Mean %

7.9 #DIV/0!

Precision - repeatability.

REQUIREMENTS SMPR

SPIFAN ERP X Checklist v 1.0

Carn-06 MEF Form

FOR ERP USE ONLY

DO NOT DISTRIBUTE