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Table 4

Product

SPIFAN Code

Analyte

Nr. replicates (n) Conc. Level

RSD

R

REQUIREMENTS SMPR

Conc.

Level

RSD

R

Child Formula Powder

00411RF00

Total Carnetine

6 0.24 mg/100 g

9.1

X

≤ Z %

Infant Element Powder

00402RF00

Total Carnetine

6 0.02 mg/100 g

73.8

Analyte 1

Adult Nut. RFT High Protein

00415RF00

Total Carnetine

6 0.04 mg/100 g

17.1

Analyte 2

Adult Nut. RFT High Fat

00407RF00

Total Carnetine

6 0.05 mg/100 g

10.1

Analyte 3

Infant Formula RFT, Milk Based Spifan Blank Milk Form Total Carnetine

6 2.69 mg/100 g

2.0

Analyte 4

SRM 1849a

CLC10-b

Total Carnetine

6 15.18 mg/100 g

2.3

Analyte 5

Adult Nut. Protein Based

11750017V3

Total Carnetine

6 0.09 mg/100 g

30.2

Analyte 1

Infant Formula, Part. Hyd. Milk

1172572116 Total Carnetine

6 10.53 mg/100 g

3.2

Analyte 2

Infant Formula, Part. Hyd. Soy

117257651Z

Total Carnetine

6 9.33 mg/100 g

1.8

Analyte 3

Adult Nut. Low Fat

00394RF00

Total Carnetine

6 0.33 mg/100 g

17.0

Analyte 4

Child Formula

000412RF00

Total Carnetine

6 49.05 mg/100 g

1.9

Analyte 5

Infant Elemental

000403RF00

Total Carnetine

6 13.74 mg/100 g

2.0

Analyte 1

Infant Formula, Milk Based

D04HTCVV

Total Carnetine

6 15.91 mg/100 g

1.8

Analyte 2

Infant Formula, Soy Based

E29JVLV

Total Carnetine

6 8.28 mg/100 g

3.5

Analyte 3

Infant Formula RFT, Milk Based Spifan Control Milk Form Total Carnetine

6 2.79 mg/100 g

1.5

Analyte 4

Adult Nut. RFT High Protein

000414RF00

Total Carnetine

6 15.62 mg/100 g

0.8

Analyte 5

Adult Nut. RFT High Fat

00406RF00

Total Carnetine

6 22.17 mg/100 g

1.2

Analyte 1

Child Formula Powder

00411RF00

Free Carnetine

6 0.15 mg/100 g

10.3

Analyte 2

Infant Element Powder

00402RF00

Free Carnetine

6 0.04 mg/100 g

38.7

Analyte 3

Adult Nut. RFT High Protein

00415RF00

Free Carnetine

6 0.04 mg/100 g

9.9

Analyte 4

Adult Nut. RFT High Fat

00407RF00

Free Carnetine

6 0.05 mg/100 g

19.0

Analyte 5

Infant Formula RFT, Milk Based Spifan Blank Milk Form Free Carnetine

6 2.51 mg/100 g

2.1

SRM 1849a

CLC10-b

Free Carnetine

6 13.08 mg/100 g

2.7

Adult Nut. Protein Based

11750017V3

Free Carnetine

6 0.07 mg/100 g

12.4

Infant Formula, Part. Hyd. Milk

1172572116 Free Carnetine

6 8.19 mg/100 g

2.7

Infant Formula, Part. Hyd. Soy

117257651Z

Free Carnetine

6 9.18 mg/100 g

2.3

Adult Nut. Low Fat

00394RF00

Free Carnetine

6 0.21 mg/100 g

11.0

Child Formula

000412RF00

Free Carnetine

6 48.45 mg/100 g

0.7

Infant Elemental

000403RF00

Free Carnetine

6 13.57 mg/100 g

1.3

Infant Formula, Milk Based

D04HTCVV

Free Carnetine

6 13.85 mg/100 g

1.7

Infant Formula, Soy Based

E29JVLV

Free Carnetine

6 8.16 mg/100 g

1.7

Infant Formula RFT, Milk Based Spifan Control Milk Form Free Carnetine

6 2.60 mg/100 g

1.4

Adult Nut. RFT High Protein

000414RF00

Free Carnetine

6 15.26 mg/100 g

2.5

Precision - reproducibility

SPIFAN ERP Checklist v 1.0

Carn-06 MEF Form

FOR ERP USE ONLY

DO NOT DISTRIBUTE