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Table 1

Accuracy - Spike Recovery

Avg (%) n=4

RSD % Avg (%) n=2 RSD (%)

Child Formula Powder

00412RF00

Trans Vitamin K

1

6

98.2

5.9

96.2

7.1

Infant Elemental Powder

00403RF00

Trans Vitamin K

1

6

93.2

7.6

94.0

2.6

SRM 1849a

CLC10-b

Trans Vitamin K

1

6

104.0

2.9

95.5

1.8

Adult Nutritional Powder Milk Protein Based

11750017V3

Trans Vitamin K

1

6

96.4

2.0

95.1

1.8

Infant Formula Powder Partially Hydrolyzed Milk Based

1172572116

Trans Vitamin K

1

6

96.6

3.6

91.9

3.0

Infant Formula Powder Partially Hydrolyzed Soy Based

117257651Z

Trans Vitamin K

1

6

97.9

1.0

96.1

2.6

Adult Nutritional Powder Low Fat

00394RF00

Trans Vitamin K

1

6

98.0

2.5

95.2

2.6

Infant Formula Powder Milk Based

D04HTCVV

Trans Vitamin K

1

6

97.6

1.0

101.8

2.3

Infant Formula Powder Soy Based

E29JVLV

Trans Vitamin K

1

6

97.9

1.7

101.8

0.3

Infant Formula RTF Milk Based

SPIFAN Control Milk Form Trans Vitamin K

1

6

100.3

1.3

104.0

0.4

Adult Nutritional RTF High Protein

00414RF00

Trans Vitamin K

1

6

96.7

2.7

106.1

0.7

Adult Nutritional RTF High Fat

00406RF00

Trans Vitamin K

1

6

98.2

1.2

93.8

4.0

Global Mean %

97.9

2.8

97.6

2.4

+ Spike Level 2 (~50%)

Spike Recovery

Product

Nr. replicates (n)

Native level

(mcg/100g

liquid)

SPIFAN Code

Analyte

+ Spike Level 1 (~100%)

SPIFAN ERP Checklist v1.0