Background Image
Table of Contents Table of Contents
Previous Page  532-533 / 620 Next Page
Information
Show Menu
Previous Page 532-533 / 620 Next Page
Page Background

Table 1

Accuracy - Spike Recovery

Avg (%)

RSD % Avg (%)

RSD (%)

Adult Nutritional RTF High Fat, placebo

00820RF00

Total B1

3 days x 2 reps

0.3

94.9

4.9

93.4

5.8

Adult Nutritional RTF High Protein, placebo

00821RF00

Total B1

3 days x 2 reps

0.4

97.7

4.3

95.4

5.5

Child Formula Powder, placebo

00847RF00

Total B1

3 days x 2 reps

1.0

99.1

5.7

97.0

7.0

Infant Elemantal Powder, placebo

00796RF

Total B1

3 days x 2 reps

0.1

93.7

6.4

92.4

7.8

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z

Total B1

3 days x 2 reps

73.5

100.2

1.8

100.8

1.8

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z

Total B1

3 days x 2 reps

74.6

101.1

1.7

102.5

1.2

Infant Formula Powder Soy Based

E10NWZC

Total B1

3 days x 2 reps

98.6

98.7

0.7

94.5

1.5

Infant Formula RTF Milk Based, placebo

EV4H2Q

Total B1

3 days x 2 reps

3.3

96.9

4.3

95.6

6.1

MEAN

97.8

3.7

96.4

4.6

Adult Nutritional RTF High Fat, placebo

00820RF00

Total B2

3 days x 2 reps

48.7

97.2

1.6

95.6

1.7

Adult Nutritional RTF High Protein, placebo

00821RF00

Total B2

3 days x 2 reps

41.2

96.5

2.3

98.4

2.7

Child Formula Powder, placebo

00847RF00

Total B2

3 days x 2 reps

26.7

98.0

2.7

98.9

2.8

Infant Elemantal Powder, placebo

00796RF

Total B2

3 days x 2 reps

6.2

95.1

1.8

96.7

1.0

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z

Total B2

3 days x 2 reps

159.0

99.9

1.8

99.7

2.4

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z

Total B2

3 days x 2 reps

101.0

100.2

2.0

99.6

1.9

Infant Formula Powder Soy Based

E10NWZC

Total B2

3 days x 2 reps

125.0

97.3

2.9

95.4

2.6

Infant Formula RTF Milk Based, placebo

EV4H2Q

Total B2

3 days x 2 reps

53.3

100.7

1.8

97.9

3.2

MEAN

98.1

2.1

97.8

2.3

Adult Nutritional RTF High Fat, placebo

00820RF00

Total B3

3 days x 2 reps

34.2

102.1

7.8

103.1

6.8

Adult Nutritional RTF High Protein, placebo

00821RF00

Total B3

3 days x 2 reps

24.4

101.7

5.9

102.9

3.8

Child Formula Powder, placebo

00847RF00

Total B3

3 days x 2 reps

10.4

105.4

6.3

105.7

5.3

Infant Elemantal Powder, placebo

00796RF

Total B3

3 days x 2 reps

5.7

104.5

6.8

103.8

4.9

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z

Total B3

3 days x 2 reps

775.0

103.0

1.8

110.7

2.4

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z

Total B3

3 days x 2 reps

787.0

102.3

2.1

105.6

2.4

Infant Formula Powder Soy Based

E10NWZC

Total B3

3 days x 2 reps

843.0

101.8

1.6

100.3

3.3

Infant Formula RTF Milk Based, placebo

EV4H2Q

Total B3

3 days x 2 reps

23.2

105.3

5.8

103.4

7.0

MEAN

103.2

4.8

104.4

4.5

Adult Nutritional RTF High Fat, placebo

00820RF00

Total B6

3 days x 2 reps

4.6

100.2

3.2

99.5

2.7

Adult Nutritional RTF High Protein, placebo

00821RF00

Total B6

3 days x 2 reps

6.3

96.8

2.4

98.9

2.7

Child Formula Powder, placebo

00847RF00

Total B6

3 days x 2 reps

6.0

99.7

1.8

99.1

1.9

Infant Elemantal Powder, placebo

00796RF

Total B6

3 days x 2 reps

1.0

98.0

2.1

98.4

3.4

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z

Total B6

3 days x 2 reps

54.4

99.1

1.3

100.1

2.4

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z

Total B6

3 days x 2 reps

56.1

100.1

2.5

100.5

2.6

Infant Formula Powder Soy Based

E10NWZC

Total B6

3 days x 2 reps

58.8

99.3

1.5

97.6

2.5

Infant Formula RTF Milk Based, placebo

EV4H2Q

Total B6

3 days x 2 reps

3.3

98.6

2.8

99.6

3.8

MEAN

99.0

2.2

99.2

2.8

Additional information to be completed by SD

yes

no

yes

yes

no

no

yes

yes

no

High (~200% Fort.)

Spike Recovery

Product

Nr. replicates (n)

Native level

ug/100g as RTF

Analyte

Low (~50% Fort.)

SPIFAN Code

Was a portion of the product spiked?

Were all spike recovery samples taken from the same spiked product?

Were multiple portions of the product spiked and each spiked product analyzed?

What percentage of the spiked sample was the spiked was the spike blanc? (How much was product diluted by spike?)

water

3% low-13% high

Mixed std

Were products spiked before they were weighed into extraction vessels?

Were all spike recovery samples prepared on multiple days?

Were spike recoveries calculated from theoretical additions?

Or was spiking solution analyzed and the results used to calculate spike recoveries?

Were all spike recovery samples prepared on the same day?

What form of the nutrient was spiked into the product?

What kind of solution or solvent was used to deliver the spike to the product?

Were products weighed into extraction vessels before spiking?

SPIFAN ERP Checklist v1.0

BVit-02 - MEF FORM

FOR ERP USE ONLY

DO NOT DISTRIBUTE