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CODEX STAN 234-1999

46

Performance characteristics of suggested methods

Provision

ML

Applicable range-from:

LOD

RSDR (%)

Recovery (%)

Suggested methods

Principle

Surface active agents

-

0.05 – 5.0 mg/L

0.05 mg/l

< 44

70-100

ISO 16265

CFA

Mineral oil

(hydrocarbon index)

-

>0.1 mg/L

< 41

71-102

ISO 9377-2

GC

PCB

-

>15 ng/L

<20

70-130

AOAC 990.06

GC ECD

Pesticide (organochlorine)

-

> 15 ng/ L

<20

70-130

AOAC 990.06

GC ECD

PAH

-

0.005 μg/L

0.04 μg/L

0.005 μg/L

<10

<18

<19

80-110

80-110

80-100

ISO 17993

ISO 7981-1

ISO 7981-2

HPLC FD

TLC

HPLC

Processed Fruits and Vegetables

Commodity

Provision

Method

Principle

Type

Processed fruits and vegetables

Benzoic acid

NMKL 124

Liquid Chromatography

II

Processed fruits and vegetables

Benzoic acid

NMKL 103; or AOAC 983.16

Gas Chromatography

III

Processed fruits and vegetables

Calcium

AOAC 968.31

Complexometry/ Titrimetry

II

Processed fruits and vegetables

Drained Weight

AOAC 968.30

(Codex General Method)

Sieving

Gravimetry

I

Processed fruits and vegetables

Fill of containers

CAC/RM 46 (reference to “metal

containers” deleted and refer to ISO 90-1

for determination of water capacity in metal

containers)

Weighing

I

Processed fruits and vegetables

Lead

AOAC 972.25 (Codex general method)

AAS (Flame absorption)

III

Processed fruits and vegetables

Packing medium

Canned berry fruits

(raspberry, strawberry)

AOAC 932.12

ISO 2173

Refractometry

I

Processed fruits and Vegetables

(except canned bamboo shoots, pH

determined by AOAC 981.12)

pH

ISO 1842

Potentiometry

IV

92